苯并[c]苯并吡喃-6-酮合成路线 （共 157 条）
反应条件
bei der Destillation;
参考文献
Graebe
Chemische Berichte, 1903 , vol. 36, p. 213 Anm.
反应条件
1: aq. NaOH solution / anschliessend Ansaeuern 2: aqueous sodium dithionite solution View Scheme
参考文献
Kenner et al.
Tetrahedron, 1957 , vol. 1, p. 259,267
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 28, p. 290
Justus Liebigs Annalen der Chemie, , vol. 284, p. 308
Justus Liebigs Annalen der Chemie, , vol. 317, p. 323
反应条件
lithium aluminium tetrahydride in diethyl ether 3.5 h; Heating;
参考文献
Ruhland, Klaus; Brueck, Andreas; Herdtweck, Eberhardt
European Journal of Inorganic Chemistry, 2007 , # 7 p. 944 - 964
反应条件
nitric acid 70 deg C, 2 h; Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 842 - 848
反应条件
oxygen; benzaldehyde; NiI2; Dowex 50W; iron powder in 1,2-dichloro-ethane
T=20°C; Baeyer-Villiger oxidation; 3 h;
参考文献
Hashemi; Beni
Journal of Chemical Research - Part S, 2000 , # 4 p. 196 - 197
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=90°C; Suzuki-Miyaura Coupling; 4 h; Inert atmosphere; Reagent/catalystTemperatureSolvent;
参考文献
Singha, Raju; Roy, Soumyabrata; Nandi, Sukla; Ray, Priyanka; Ray, Jayanta K.
Tetrahedron Letters, 2013 , vol. 54, # 7 p. 657 - 660
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=90°C; Suzuki-Miyaura Coupling; 8 h; Inert atmosphere; Reagent/catalystTemperatureSolvent;
参考文献
Singha, Raju; Roy, Soumyabrata; Nandi, Sukla; Ray, Priyanka; Ray, Jayanta K.
Tetrahedron Letters, 2013 , vol. 54, # 7 p. 657 - 660
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=90°C; Suzuki-Miyaura Coupling; 3 h; Inert atmosphere; Reagent/catalystTemperatureSolvent;
参考文献
Singha, Raju; Roy, Soumyabrata; Nandi, Sukla; Ray, Priyanka; Ray, Jayanta K.
Tetrahedron Letters, 2013 , vol. 54, # 7 p. 657 - 660
反应条件
oxygen; copper diacetate; palladium diacetate; sodium carbonate; 1,3,5-trimethyl-benzene; 2,2,2-trimethylacetic acid
T=120°C; P=760.051 Torr; 6 h; Schlenk techniqueSealed tube; TimeReagent/catalystConcentration;
参考文献
Luo, Shuang; Luo, Fei-Xian; Zhang, Xi-Sha; Shi, Zhang-Jie
Angewandte Chemie - International Edition, 2013 , vol. 52, # 40 p. 10598 - 10601
Angew. Chem., 2013 , vol. 125, # 40 p. 10792 - 10795,4
