苯并[c]苯并吡喃-6-酮合成路线 （共 157 条）
反应条件
1: potassium carbonate / acetone / 50 °C
2: 2,9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 24 h / 100 °C / Inert atmosphere
3: pyridinium chlorochromate / dichloromethane / 20 °C
View Scheme
参考文献
Sun, Chang-Liang; Gu, Yi-Fan; Huang, Wei-Ping; Shi, Zhang-Jie
Chemical Communications, 2011 , vol. 47, # 35 p. 9813 - 9815
反应条件
1: 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
2: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl acetamide / 1.5 h / 150 °C / Inert atmosphere
View Scheme
参考文献
Hong, Lisa P. T.; White, Jonathan M.; Donner, Christopher D.
Australian Journal of Chemistry, 2012 , vol. 65, # 1 p. 58 - 64
反应条件
1: water / 60 - 150 °C / |Microwave irradiation
2: dihydrogen peroxide / water; ethanol / 40 - 80 °C / |Microwave irradiation
View Scheme
参考文献
He, Yan; Zhang, Xinying; Cui, Liangyan; Wang, Jianji; Fan, Xuesen
Green Chemistry, 2012 , vol. 14, # 12 p. 3429 - 3435
反应条件
1: Jone's reagent / acetone / 0 °C
2: silver nitrate / acetonitrile / 1.5 h / 80 °C
3: water / 60 - 150 °C / |Microwave irradiation
4: dihydrogen peroxide / water; ethanol / 40 - 80 °C / |Microwave irradiation
View Scheme
参考文献
He, Yan; Zhang, Xinying; Cui, Liangyan; Wang, Jianji; Fan, Xuesen
Green Chemistry, 2012 , vol. 14, # 12 p. 3429 - 3435
反应条件
1: zinc / N,N-dimethyl-formamide; tetrahydrofuran / 20 °C
2: Jone's reagent / acetone / 0 °C
3: silver nitrate / acetonitrile / 1.5 h / 80 °C
4: water / 60 - 150 °C / |Microwave irradiation
5: dihydrogen peroxide / water; ethanol / 40 - 80 °C / |Microwave irradiation
View Scheme
参考文献
He, Yan; Zhang, Xinying; Cui, Liangyan; Wang, Jianji; Fan, Xuesen
Green Chemistry, 2012 , vol. 14, # 12 p. 3429 - 3435
反应条件
1: silver nitrate / acetonitrile / 1.5 h / 80 °C
2: water / 60 - 150 °C / |Microwave irradiation
3: dihydrogen peroxide / water; ethanol / 40 - 80 °C / |Microwave irradiation
View Scheme
参考文献
He, Yan; Zhang, Xinying; Cui, Liangyan; Wang, Jianji; Fan, Xuesen
Green Chemistry, 2012 , vol. 14, # 12 p. 3429 - 3435
反应条件
1: palladium diacetate; triphenylphosphine; sodium acetate / N,N-dimethyl-formamide / 3 h / 80 °C
2: pyridinium chlorochromate / dichloromethane / 20 °C
View Scheme
参考文献
Ahmed, Atiur; Dhara, Shubhendu; Ray, Jayanta K.
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1673 - 1676
反应条件
1: ozone / dichloromethane / 0.67 h / -78 - 10 °C / |Cooling with acetone-dry ice
2: |Heating
View Scheme
参考文献
Bartoloni, Fernando H.; De Oliveira, Marcelo A.; Augusto, Felipe A.; Ciscato, Luiz Francisco M. L.; Bastos, Erick L.; Baader, Wilhelm J.
Journal of the Brazilian Chemical Society, 2012 , vol. 23, # 11 p. 2093 - 2103
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / tetrahydrofuran; water / 20 - 80 °C / |Schlenk technique; |Inert atmosphere
2: sodium hydroxide; water / tetrahydrofuran / 80 °C
3: dipotassium peroxodisulfate; oxygen / water; acetonitrile / 18 h / 50 °C
View Scheme
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / tetrahydrofuran; water / 20 - 80 °C / |Schlenk technique; |Inert atmosphere
2: sodium hydroxide; water / tetrahydrofuran / 80 °C
3: dipotassium peroxodisulfate; oxygen / water; acetonitrile / 18 h / 50 °C
View Scheme
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
