苯并[c]苯并吡喃-6-酮合成路线 (共 157 条)
反应条件
pyridine; tert.-butylhydroperoxide; potassium iodide in water; acetonitrile
T=80°C; 48 h; Green chemistry; Reagent/catalystTemperatureSolvent;
参考文献
Zhou, Jing; Han, Pan; Xu, Ying-Meng; Zhang, Tao; Du, Zhen-Ting
Heterocycles, 2013 , vol. 87, # 9 p. 1889 - 1896
反应条件
copper(l) iodide; sodium carbonate in N,N-dimethyl-formamide
T=25 - 200°C; 0.333333 h; microwave irradiation;
参考文献
Thasana, Nopporn; Worayuthakarn, Rattana; Kradanrat, Phithakpong; Hohn, Elliot; Young, Lauren; Ruchirawat, Somsak
Journal of Organic Chemistry, 2007 , vol. 72, # 24 p. 9379 - 9382
反应条件
copper(l) iodide; sodium carbonate in N,N-dimethyl-formamide
T=25 - 200°C; 0.333333 h; microwave irradiation;
参考文献
Thasana, Nopporn; Worayuthakarn, Rattana; Kradanrat, Phithakpong; Hohn, Elliot; Young, Lauren; Ruchirawat, Somsak
Journal of Organic Chemistry, 2007 , vol. 72, # 24 p. 9379 - 9382
反应条件
oxygen; lithium perchlorate in water; acetonitrile
Electrochemical reaction;
参考文献
Batanero, Belen; Barba, Fructuoso; Barba, Isidoro; Elinson, Michail N.
Tetrahedron Letters, 2014 , vol. 55, # 1 p. 82 - 85
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=50°C; 4 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
反应条件
lead(IV) acetate; iodine in dichloromethane; benzene
T=60 - 70°C; 2 h; Irradiation;
参考文献
Muraki, Takahito; Togo, Hideo; Yokoyama, Masataka
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1713 - 1716
反应条件
[BMIM][Al2Cl7] in dichloromethane
20 h; Heating;
参考文献
Kemperman, Gerardus J.; Ter Horst; Van De Goor; Roeters; Bergwerff; Van Der Eem; Basten
European Journal of Organic Chemistry, 2006 , # 14 p. 3169 - 3174
反应条件
palladium diacetate; sodium acetate in N,N-dimethyl-formamide
1 h; Heating;
参考文献
Harayama, Takashi; Yasuda, Hirotake; Akiyama, Toshihiko; Takeuchi, Yasuo; Abe, Hitoshi
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 6 p. 861 - 864
反应条件
palladium diacetate in methanol; dimethyl sulfoxide
T=25°C; 3 h;
参考文献
Zhou, Q. Jean; Worm, Karin; Dolle, Roland E.
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5147 - 5149
反应条件
1: (+/-)-(6aS,10R,10aR)-10-(1,1-dimethylethyl)dimethylsilyloxy-6-oxo-6a,7,10,10a-tetrahydro-6H-benzo[c]chromene-10a-carbonitrile With N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium; diisopropylamine in tetrahydrofuran
T=-78°C; 0.5 h; Inert atmosphere;
2: methyl iodide in tetrahydrofuran
T=-78 - -40°C; 2 h; Inert atmosphere;
参考文献
Jung, Michael E.; Allen, Damian A.
Organic Letters, 2009 , vol. 11, # 3 p. 757 - 760