苯并[c]苯并吡喃-6-酮合成路线 （共 157 条）
反应条件
TEMPO; oxygen in acetonitrile
T=50°C; P=760.051 Torr; 96 h;
参考文献
Song, Ren-Jie; Liu, Yu; Hu, Rui-Xiang; Liu, Yan-Yun; Wu, Ji-Cheng; Yang, Xu-Heng; Li, Jin-Heng
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1467 - 1473
反应条件
palladium diacetate; sodium acetate; triphenylphosphine in N,N-dimethyl-formamide
2 h; Heating;
参考文献
Harayama, Takashi; Yasuda, Hirotake
Heterocycles, 1997 , vol. 46, # 1 p. 61 - 64
反应条件
pyridinium chlorochromate in dichloromethane
T=20°C;
参考文献
Ahmed, Atiur; Dhara, Shubhendu; Ray, Jayanta K.
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1673 - 1676
反应条件
t-BuOI in tert-butyl alcohol
T=25°C; 3 h; Irradiation;
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 842 - 848
反应条件
bis(acetylacetonato) palladium; potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether; copper(l) chloride in 1-methyl-pyrrolidin-2-one
T=165°C; 16 h; Inert atmosphereMolecular sieve; chemoselective reaction;
参考文献
Luo, Jiaying; Lu, Youling; Liu, Saiwen; Liu, Jing; Deng, Guo-Jun
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2604 - 2608
反应条件
bis(acetylacetonato) palladium; potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether; copper(l) chloride in 1-methyl-pyrrolidin-2-one
T=165°C; 16 h; Inert atmosphereMolecular sieve; chemoselective reaction;
参考文献
Luo, Jiaying; Lu, Youling; Liu, Saiwen; Liu, Jing; Deng, Guo-Jun
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2604 - 2608
反应条件
bis(acetylacetonato) palladium; potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether; copper(l) chloride in 1-methyl-pyrrolidin-2-one
T=165°C; 16 h; Inert atmosphereMolecular sieve; chemoselective reaction;
参考文献
Luo, Jiaying; Lu, Youling; Liu, Saiwen; Liu, Jing; Deng, Guo-Jun
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2604 - 2608
反应条件
t-BuOI in tert-butyl alcohol
T=25°C; 3 h; Irradiation;
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 842 - 848
反应条件
iodine; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane; benzene
T=60 - 70°C; 2 h; Irradiation;
参考文献
Togo, Hideo; Muraki, Takahito; Yokoyama, Masataka
Tetrahedron Letters, 1995 , vol. 36, # 39 p. 7089 - 7092
反应条件
1: 86 percent / (2,6-iPr2-C6H3OCO-N)-imidazolium-(N-CH2C6H4-2-Br) bromide; Cs2CO3; (t-Bu)2PH / Pd2dba3 / dioxane / 48 h / 150 °C
2: 91 percent / BBr3 / CH2Cl2 / 3 h / -78 - 20 °C
View Scheme
参考文献
Palencia, Hector; Garcia-Jimenez, Federico; Takacs, James M.
Tetrahedron Letters, 2004 , vol. 45, # 20 p. 3849 - 3853
