苯并[c]苯并吡喃-6-酮合成路线 （共 157 条）
反应条件
iodine; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane; benzene
T=60 - 70°C; 2 h; Irradiation;
参考文献
Togo, Hideo; Muraki, Takahito; Yokoyama, Masataka
Tetrahedron Letters, 1995 , vol. 36, # 39 p. 7089 - 7092
反应条件
1: 99 percent / Na2CO3; Pd(OAc)2; triphenylphosphane / [BMIM][Cl] / toluene; H2O / 3.5 h / Heating
2: 93 percent / [BMIM][Al2Cl7] / CH2Cl2 / 20 h / Heating
View Scheme
参考文献
Kemperman, Gerardus J.; Ter Horst; Van De Goor; Roeters; Bergwerff; Van Der Eem; Basten
European Journal of Organic Chemistry, 2006 , # 14 p. 3169 - 3174
反应条件
1: 99 percent / BCl3 / AlCl3 / hexane / 6 h / 70 °C
2: 90 percent / Pd(OAc)2 / dimethylsulfoxide; methanol / 3 h / 25 °C
View Scheme
参考文献
Zhou, Q. Jean; Worm, Karin; Dolle, Roland E.
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5147 - 5149
反应条件
sulfolane; potassium dihydrogenphosphate; tert-butyl XPhos; tetrabutylammomium bromide; copper diacetate; palladium diacetate
T=150°C; 16 h; Molecular sieve;
参考文献
Cant, Alastair A.; Roberts, Lee; Greaney, Michael F.
Chemical Communications, 2010 , vol. 46, # 45 p. 8671 - 8673
反应条件
t-BuOI in tert-butyl alcohol
T=25°C; 7 h; Irradiation;
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 842 - 848
反应条件
dipotassium peroxodisulfate; trifluoroacetic acid; Pd(PCOCF3)2
T=80°C; 70 h; Further byproducts given;
参考文献
Shibahara, Fumitoshi; Kinoshita, Shinsuke; Nozaki, Kyoko
Organic Letters, 2004 , vol. 6, # 14 p. 2437 - 2439
反应条件
1: 99 percent / BCl3 / AlCl3 / hexane / 6 h / 70 - 75 °C
2: 90 percent / Pd(OAc)2 / dimethylsulfoxide; methanol / 3 h / 25 °C
View Scheme
参考文献
Zhou, Q. Jean; Worm, Karin; Dolle, Roland E.
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5147 - 5149
反应条件
iodine; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane
5 h; Ambient temperatureIrradiation;
参考文献
Togo, Hideo; Muraki, Takahito; Yokoyama, Masataka
Tetrahedron Letters, 1995 , vol. 36, # 39 p. 7089 - 7092
反应条件
bis-triphenylphosphine-palladium(II) chloride; pivalic acid sodium salt in N,N-dimethyl acetamide
T=80°C; 10 h; Heating;
参考文献
Harayama, Takashi; Yasuda, Hirotake
Heterocycles, 1997 , vol. 46, # 1 p. 61 - 64
反应条件
1: 99 percent / Na2CO3; Pd(OAc)2; triphenylphosphane / [BMIM][Cl] / toluene; H2O / 3.5 h / Heating
2: 93 percent / [BMIM][Al2Cl7] / CH2Cl2 / 20 h / Heating
View Scheme
参考文献
Kemperman, Gerardus J.; Ter Horst; Van De Goor; Roeters; Bergwerff; Van Der Eem; Basten
European Journal of Organic Chemistry, 2006 , # 14 p. 3169 - 3174
