苯并[c]苯并吡喃-6-酮合成路线 （共 157 条）
反应条件
bis(acetylacetonato) palladium; potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether; copper(l) chloride in 1-methyl-pyrrolidin-2-one
T=165°C; 16 h; Inert atmosphereMolecular sieve; chemoselective reaction;
参考文献
Luo, Jiaying; Lu, Youling; Liu, Saiwen; Liu, Jing; Deng, Guo-Jun
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2604 - 2608
反应条件
tetrahydrofuran; carbon dioxide; lithium
anschliessende Hydrolyse;
参考文献
Gilman; Dietrich
Journal of Organic Chemistry, 1957 , vol. 22, p. 851
反应条件
t-BuOI in tert-butyl alcohol
T=25°C; 4.3 h; Irradiation;
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 842 - 848
反应条件
1: CsF / acetonitrile / 10 h / 20 °C
2: tricyclohexylphosphine / Pd(OAc)2 / acetonitrile / 24 h / 100 °C
View Scheme
参考文献
Liu, Zhijian; Larock, Richard C.
Tetrahedron, 2007 , vol. 63, # 2 p. 347 - 355
反应条件
1: CsF / acetonitrile / 10 h / 20 °C
2: tricyclohexylphosphine / Pd(OAc)2 / acetonitrile / 24 h / 100 °C
View Scheme
参考文献
Liu, Zhijian; Larock, Richard C.
Tetrahedron, 2007 , vol. 63, # 2 p. 347 - 355
反应条件
1: 1.) Merrifield resin, Na; 2.) aq. Na2CO3; 3.) aq. HCl / 2.) Pd(PPh3)4 / 2.) DME, reflux, 48 h; 3.) dioxan, 80 deg C, 48 h
2: LiAlH4
3: CrO3 in H2SO4 / acetone
View Scheme
参考文献
Chamoin; Houldsworth; Kruse; Bakker, W. Iwema; Snieckus
Tetrahedron Letters, 1998 , vol. 39, # 24 p. 4179 - 4182
反应条件
antimony(V) pentachloride
T=20°C; 0.666667 h; other reagent, time; Product distribution;
参考文献
Miura, Masahiro; Nojima, Masamoto; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1950 - 1954
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
参考文献
Motherwell, William B.; Pennell, Andrew M. K.
Journal of the Chemical Society, Chemical Communications, 1991 , # 13 p. 877 - 879
反应条件
hydrogen iodide; acetic anhydride
1 h; Heating;
参考文献
Hattori, Tetsutaro; Suzuki, Takatsugu; Hayashizaka, Noriyuki; Koike, Nobuyuki; Miyano, Sotaro
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 3034 - 3040
反应条件
copper(l) iodide; 1,10-phenanthroline; palladium diacetate; potassium carbonate in 1-methyl-pyrrolidin-2-one
T=160°C; 16 h; Inert atmosphereMolecular sieve; chemoselective reaction;
参考文献
Luo, Jiaying; Lu, Youling; Liu, Saiwen; Liu, Jing; Deng, Guo-Jun
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2604 - 2608
