苯并[c]苯并吡喃-6-酮合成路线 （共 157 条）
反应条件
2,2'-azo-bisisobutyronitrile; diphenyl diselenide; tri-n-butyl-tin hydride in benzene
1 h; Heatingother reagent: Bu3SnH/azobis(isobutyronitrile); Further byproducts given;
参考文献
Crich, David; Hwang, Jae-Taeg
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2765 - 2770
反应条件
1: 87 percent / pyridine
2: 34 percent / AIBN; (Me3Si)3SiH / benzene / 80 °C
View Scheme
参考文献
Zhang, Wei; Pugh, Georgia
Tetrahedron Letters, 2001 , vol. 42, # 33 p. 5613 - 5615
反应条件
water; oxygen; P-25 TiO2 in acetonitrile
T=20°C; 76 h; UV-irradiation; Product distribution; Further Variations:reaction time;
参考文献
Higashida, Suguru; Harada, Aiko; Kawakatsu, Rikako; Fujiwara, Noriko; Matsumura, Michio
Chemical Communications, 2006 , # 26 p. 2804 - 2806
反应条件
1: palladium diacetate; triphenylphosphine; sodium acetate / N,N-dimethyl-formamide / 3 h / 80 °C
2: pyridinium chlorochromate / dichloromethane / 20 °C
View Scheme
参考文献
Ahmed, Atiur; Dhara, Shubhendu; Ray, Jayanta K.
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1673 - 1676
反应条件
sulfuric acid; dihydrogen peroxide; acetic acid
Ambient temperature;
参考文献
Taljaard, Benjamin; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 931 - 934
反应条件
thionyl chloride
T=4°C; 0.416667 h; Title compound not separated from byproducts;
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 842 - 848
参考文献
Caswell, Michael; Schmir, Gaston L.
Journal of the American Chemical Society, 1980 , vol. 102, # 14 p. 4815 - 4821
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
1 h; Heatingother reagent: Bu3SnH/azobis(isobutyronitrile)/diphenyl diselenide; Further byproducts given;
参考文献
Crich, David; Hwang, Jae-Taeg
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2765 - 2770
反应条件
palladium diacetate; sodium acetate; triphenylphosphine in N,N-dimethyl-formamide
Arylation; 2 h; Heating;
参考文献
Harayama, Takashi; Yasuda, Hirotake; Akiyama, Toshihiko; Takeuchi, Yasuo; Abe, Hitoshi
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 6 p. 861 - 864
反应条件
1: potassium carbonate / acetone / 50 °C
2: 2,9-dimethyl-1,10-phenanthroline; potassium tert-butylate / 1,4-dioxane / 24 h / 100 °C / Inert atmosphere
3: pyridinium chlorochromate / dichloromethane / 20 °C
View Scheme
参考文献
Sun, Chang-Liang; Gu, Yi-Fan; Huang, Wei-Ping; Shi, Zhang-Jie
Chemical Communications, 2011 , vol. 47, # 35 p. 9813 - 9815
