苯并[c]苯并吡喃-6-酮合成路线 （共 157 条）
反应条件
dibenzoyl peroxide
T=60°C; 3 h;
参考文献
Auricchio, Sergio; Citterio, Attilio; Sebastiano, Roberto
Journal of Organic Chemistry, 1990 , vol. 55, # 26 p. 6312 - 6316
反应条件
oxygen in acetonitrile
Decomposition; Irradiationphotolysis;
参考文献
Karatsu, Takashi; Yoshita, Yasuhiro; Fukui, Keijiro; Kitamura, Akihide
Chemistry Letters, 1999 , # 9 p. 877 - 878
反应条件
2: aq. NaClO2, H2O2 / acetonitrile
3: (COCl)2
5: 22 percent / Pd(PPh3)2Cl2, NaOPiv / N,N-dimethyl-acetamide / 10 h / 80 °C / Heating
View Scheme
参考文献
Harayama, Takashi; Yasuda, Hirotake
Heterocycles, 1997 , vol. 46, # 1 p. 61 - 64
反应条件
1: aq. NaClO2, H2O2 / acetonitrile
2: (COCl)2
4: 22 percent / Pd(PPh3)2Cl2, NaOPiv / N,N-dimethyl-acetamide / 10 h / 80 °C / Heating
View Scheme
参考文献
Harayama, Takashi; Yasuda, Hirotake
Heterocycles, 1997 , vol. 46, # 1 p. 61 - 64
反应条件
1: (COCl)2
3: 22 percent / Pd(PPh3)2Cl2, NaOPiv / N,N-dimethyl-acetamide / 10 h / 80 °C / Heating
View Scheme
参考文献
Harayama, Takashi; Yasuda, Hirotake
Heterocycles, 1997 , vol. 46, # 1 p. 61 - 64
反应条件
1: 98 percent / diethyl ether; benzene / 1 h / Ambient temperature
2: 81 percent / acetic anhydride, aq. HI / 1 h / Heating
View Scheme
参考文献
Hattori, Tetsutaro; Suzuki, Takatsugu; Hayashizaka, Noriyuki; Koike, Nobuyuki; Miyano, Sotaro
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 3034 - 3040
反应条件
1: 98 percent / diethyl ether; benzene / 1 h / Ambient temperature
2: 81 percent / acetic anhydride, aq. HI / 1 h / Heating
View Scheme
参考文献
Hattori, Tetsutaro; Suzuki, Takatsugu; Hayashizaka, Noriyuki; Koike, Nobuyuki; Miyano, Sotaro
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 3034 - 3040
反应条件
1: 73 percent / triluoroacetic anhydride / 4 h / Ambient temperature
2: 98 percent / diethyl ether; benzene / 1 h / Ambient temperature
3: 81 percent / acetic anhydride, aq. HI / 1 h / Heating
View Scheme
参考文献
Hattori, Tetsutaro; Suzuki, Takatsugu; Hayashizaka, Noriyuki; Koike, Nobuyuki; Miyano, Sotaro
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 10 p. 3034 - 3040
反应条件
1: 10 percent / xylene / 130 °C
2: silica, H2O
View Scheme
参考文献
Le Roux, Jean-Pierre; Desbene, Paul-Louis; Cherton, Jean-Claude
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 847 - 849
反应条件
18-crown-6 ether in benzene
24 h; Ambient temperature;
参考文献
Forrester, Alexander R.; Purushotham, Vemeshetti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 945 - 951
