苯并[c]苯并吡喃-6-酮合成路线 （共 157 条）
反应条件
in toluene
21.5 h; Heating;
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 842 - 848
反应条件
1: air; SiO2 / 65 h / Photolysis
2: air; SiO2 / Photolysis
View Scheme
参考文献
Barbas, John T.; Sigman, Michael E.; Dabestani, Reza
Environmental Science and Technology, 1996 , vol. 30, # 5 p. 1776 - 1780
反应条件
1: 76.9 percent / conc. HCl, Zn powder / H2O; acetic acid / 5 h / 5 °C
2: 1.) NaNO2; 2.) Gattermann copper powder / 1.) H2O, 0.5 N H2SO4, 0 deg C
3: O2 / 168 h
View Scheme
参考文献
Majumder; Sarkar
Journal of the Indian Chemical Society, 1989 , vol. 66, # 8-10 p. 673 - 680
反应条件
1: 1.9 g / K2CO3 / methanol / 5 h / Heating
2: 76.9 percent / conc. HCl, Zn powder / H2O; acetic acid / 5 h / 5 °C
3: 1.) NaNO2; 2.) Gattermann copper powder / 1.) H2O, 0.5 N H2SO4, 0 deg C
4: O2 / 168 h
View Scheme
参考文献
Majumder; Sarkar
Journal of the Indian Chemical Society, 1989 , vol. 66, # 8-10 p. 673 - 680
反应条件
1: 1.9 g / K2CO3 / methanol / 5 h / Heating
2: 76.9 percent / conc. HCl, Zn powder / H2O; acetic acid / 5 h / 5 °C
3: 1.) NaNO2; 2.) Gattermann copper powder / 1.) H2O, 0.5 N H2SO4, 0 deg C
4: O2 / 168 h
View Scheme
参考文献
Majumder; Sarkar
Journal of the Indian Chemical Society, 1989 , vol. 66, # 8-10 p. 673 - 680
反应条件
1: KOH / ethanol
2: 57 percent / t-butyl hypoiodite / 2-methyl-propan-2-ol / 3 h / 25 °C / Irradiation
View Scheme
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 842 - 848
反应条件
1: 18-crown-6 / acetonitrile / 24 h / Heating
2: KOH / ethanol
3: 57 percent / t-butyl hypoiodite / 2-methyl-propan-2-ol / 3 h / 25 °C / Irradiation
View Scheme
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 842 - 848
反应条件
1: 2,9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 24 h / 100 °C / Inert atmosphere
2: pyridinium chlorochromate / dichloromethane / 20 °C
View Scheme
参考文献
Sun, Chang-Liang; Gu, Yi-Fan; Huang, Wei-Ping; Shi, Zhang-Jie
Chemical Communications, 2011 , vol. 47, # 35 p. 9813 - 9815
反应条件
1: 2,9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 24 h / 100 °C / Inert atmosphere
2: pyridinium chlorochromate / dichloromethane / 20 °C
View Scheme
参考文献
Sun, Chang-Liang; Gu, Yi-Fan; Huang, Wei-Ping; Shi, Zhang-Jie
Chemical Communications, 2011 , vol. 47, # 35 p. 9813 - 9815
反应条件
1: 2,9-dimethyl-1,10-phenanthroline; potassium tert-butylate / benzene / 24 h / 100 °C / Inert atmosphere
2: pyridinium chlorochromate / dichloromethane / 20 °C
View Scheme
参考文献
Sun, Chang-Liang; Gu, Yi-Fan; Huang, Wei-Ping; Shi, Zhang-Jie
Chemical Communications, 2011 , vol. 47, # 35 p. 9813 - 9815
