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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴喹啉
合成路线
（共 61 条）
2005-43-8
2-溴喹啉
+
1066-54-2
三甲基乙炔基硅
→
反应条件
86521-07-5
2-(2-(三甲基甲硅烷基)乙炔)喹啉
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine T=70°C; 3 h;
参考文献
Sakamoto, Takao; Shiraiwa, Masafumi; Kondo, Yoshinori; Yamanaka, Hiroshi
Synthesis, 1983 , # 4 p. 312 - 314
2005-43-8
2-溴喹啉
→
反应条件
86814-56-4
2-溴-3-羟基喹啉
反应条件
1: With 2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran T=-78°C; 1 h; 2: With boric acid trimethyl ester in tetrahydrofuran T=-78°C; 2 h; 3: With dihydrogen peroxide; ammonium chloride in tetrahydrofuran; diethyl ether; water
参考文献
Riego, Estela; Bayo, Nuria; Cuevas, Carmen; Albericio, Fernando; Alvarez, Mercedes
Tetrahedron, 2005 , vol. 61, # 6 p. 1407 - 1411
2005-43-8
2-溴喹啉
→
反应条件
6560-83-4
2-碘喹啉
反应条件
1: With Bu3MgLi in tetrahydrofuran T=-10°C; 2 h; 2: With iodine in tetrahydrofuran T=-10°C; 1 h;
参考文献
Dumouchel, Sylvain; Mongin, Florence; Trecourt, Francois; Queguiner, Guy
Tetrahedron, 2003 , vol. 59, # 43 p. 8629 - 8640
419536-33-7
4-(9H-咔唑-9-基)苯硼酸
+
2005-43-8
2-溴喹啉
→
反应条件
901117-84-8
反应条件
palladium diacetate; potassium carbonate in ethanol; water T=80°C; Suzuki Coupling; 0.666667 h;
参考文献
Rao, Xiaofeng; Liu, Chun; Qiu, Jieshan; Jin, Zilin
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 39 p. 7875 - 7883
2005-43-8
2-溴喹啉
+
74497-02-2
→
反应条件
5468-85-9
N-苯基-2-喹啉胺
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in 1,4-dioxane T=100°C; Inert atmosphere;
参考文献
Wang, Honggen; Wang, Yong; Peng, Changlan; Zhang, Jiancun; Zhu, Qiang
Journal of the American Chemical Society, 2010 , vol. 132, # 38 p. 13217 - 13219
2005-43-8
2-溴喹啉
+
74497-02-2
→
反应条件
5468-85-9
N-苯基-2-喹啉胺
反应条件
tert-butyl N,N,N',N'-tetraisopropylphosphorodiamidite; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate in toluene T=105°C; Buchwald-Hartwig Coupling; 20 h; Inert atmosphereSchlenk technique;
参考文献
Roiban, Gheorghe-Doru; Mehler, Gerlinde; Reetz, Manfred T.
European Journal of Organic Chemistry, 2014 , vol. 2014, # 10 p. 2070 - 2076
2005-43-8
2-溴喹啉
→
反应条件
58346-55-7
反应条件
1: THF / -50 °C 2: diethyl ether / -50 °C View Scheme
参考文献
Gilman; Soddy
Journal of Organic Chemistry, 1957 , vol. 22, p. 565
2005-43-8
2-溴喹啉
+
5332-24-1
3-溴喹啉
→
反应条件
612-81-7
反应条件
1: 3-(bromo)-quinoline With (nBu)3MgLi in tetrahydrofuran; diethyl ether; hexane T=-30 - -10°C; 2: 2-bromoquinoline With 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran; diethyl ether; hexane T=-10 - 20°C; 19 h;
参考文献
Dumouchel, Sylvain; Mongin, Florence; Trecourt, Francois; Queguiner, Guy
Tetrahedron, 2003 , vol. 59, # 43 p. 8629 - 8640
2005-43-8
2-溴喹啉
→
反应条件
612-81-7
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [Pd2(dba)2] in tetrahydrofuran T=20°C; 18 h;
参考文献
Dumouchel, Sylvain; Mongin, Florence; Trecourt, Francois; Queguiner, Guy
Tetrahedron Letters, 2003 , vol. 44, # 19 p. 3877 - 3880
2005-43-8
2-溴喹啉
+
1692-25-7
吡啶-3-硼酸
→
反应条件
6294-65-1
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate T=80°C; Suzuki cross-coupling;
参考文献
Voets, Marieke; Antes, Iris; Scherer, Christiane; Mueller-Vieira, Ursula; Biemel, Klaus; Barassin, Catherine; Marchais-Oberwinkler, Sandrine; Hartmann, Rolf W.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 21 p. 6632 - 6642
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