(S)-1-(2,4,6-三甲苯基)乙胺合成路线 （共 5 条）
反应条件
hydrogenchloride in methanol Hydrolysis; 6 h; Heating;
参考文献
Kohara, Takehiro; Hashimoto, Yukihiko; Shioya, Rieko; Saigo, Kazuhiko
Tetrahedron Asymmetry, 1999 , vol. 10, # 24 p. 4831 - 4840
反应条件
1: 88 percent / Na; EtOH; liq. NH3 / tetrahydrofuran / 1 h / Heating 2: 37 percent / CH2Cl2 / 40 h / 20 °C 3: 72 percent / DIBAL / tetrahydrofuran / 40 h / 20 °C 4: 90 percent / aq. HCl / methanol / 6 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 10, # 24 p. 4831 - 4840
反应条件
1: 47 percent / CeCl3 / tetrahydrofuran / 16 h / Heating 2: 88 percent / Na; EtOH; liq. NH3 / tetrahydrofuran / 1 h / Heating 3: 37 percent / CH2Cl2 / 40 h / 20 °C 4: 72 percent / DIBAL / tetrahydrofuran / 40 h / 20 °C 5: 90 percent / aq. HCl / methanol / 6 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 10, # 24 p. 4831 - 4840
反应条件
1: 37 percent / CH2Cl2 / 40 h / 20 °C 2: 72 percent / DIBAL / tetrahydrofuran / 40 h / 20 °C 3: 90 percent / aq. HCl / methanol / 6 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 10, # 24 p. 4831 - 4840
反应条件
1: 72 percent / DIBAL / tetrahydrofuran / 40 h / 20 °C 2: 90 percent / aq. HCl / methanol / 6 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 10, # 24 p. 4831 - 4840
