(4-乙酰基苯基)乙酸甲酯合成路线 (共 7 条)
反应条件
potassium carbonate; palladium diacetate; P(o-tolyl)3 in tetrahydrofuran; water T=20°C; 19 h;
参考文献
TECHNISCHE UNIVERSITAeT MUeNCHEN; JONES, Nicholas, Andrew
Patent: WO2008/68516 A1, 2008 ;
Location in patent: Page/Page column 12-13; 26 ;
反应条件
triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane in N,N-dimethyl-formamide T=60°C;
参考文献
Garrido, Fabrice; Raeppel, Stephane; Mann, Andre; Lautens, Mark
Tetrahedron Letters, 2001 , vol. 42, # 2 p. 265 - 266
反应条件
manganese; NiBr2bipy; trifluoroacetic acid in N,N-dimethyl-formamide T=50°C; 1 h;
参考文献
Durandetti, Muriel; Gosmini, Corinne; Perichon, Jacques
Tetrahedron, 2007 , vol. 63, # 5 p. 1146 - 1153
反应条件
aluminium trichloride
参考文献
Bergmann; Blum
Journal of Organic Chemistry, 1959 , vol. 24, p. 549
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Lai; Tidwell
Journal of the American Chemical Society, 1977 , vol. 99, p. 1465,1469
反应条件
sodium tetrahydroborate
参考文献
Bergmann; Blum
Journal of Organic Chemistry, 1959 , vol. 24, p. 549
反应条件
bromine in tetrachloromethane
1 h; Ambient temperature;
参考文献
Shridhar, D. R.; Sastry, C. V. Reddy; Lal, B.; Singh, P. P.; Rao, C. Seshagiri; Junnarkar, A. Y.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 6 p. 602 - 604
参考文献
Dr. Karl Thomae GmbH
Patent: US5922717 A1, 1999 ;