2-三氟甲磺酰氧-1-萘甲酯合成路线 （共 8 条）
反应条件
pyridine in dichloromethane T=0°C; triflation; 14 h;
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
pyridine; trifluoromethanesulfonic acid anhydride in dichloromethane; toluene
反应条件
zinc; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in N,N-dimethyl-formamide T=100 - 110°C;
参考文献
Ager, David J.; East, Michael B.; Eisenstadt, Amihai; Laneman, Scott A.
Chemical Communications, 1997 , # 24 p. 2359 - 2360
反应条件
bis(benzonitrile)palladium(II) dichloride in toluene Substitution; 26 h; Heating;
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
in N,N-dimethyl-formamide
参考文献
Monsanto Company
Patent: US5874628 A1, 1999 ;
反应条件
1: 95 percent / bis(benzonitrile)palladium dichloride / toluene / 26 h / Heating 2: 88 percent / barium hydroxide octahydrate / methanol / 25 h / Heating View Scheme
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
1.1: 95 percent / bis(benzonitrile)palladium dichloride / toluene / 26 h / Heating 2.1: 88 percent / barium hydroxide octahydrate / methanol / 25 h / Heating 3.1: Et3N; diphenylchlorophosphite / CH2Cl2 / 5 h / 0 - 20 °C 3.2: 51 percent / DMAP / CH2Cl2 / 12 h / 25 °C View Scheme
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris(dibenzylideneacetone)dipalladium (0); ZnF2 in N,N-dimethyl-formamide
T=150°C; 0.25 h; Irradiationmicrowave;
参考文献
Chobanian, Harry R.; Liu, Ping; Chioda, Marc D.; Guo, Yan; Lin, Linus S.
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1213 - 1216
