1-(甲氧基甲基)-1H-咪唑合成路线 （共 4 条）
反应条件
1: 1H-imidazole With sodium hydride in tetrahydrofuran; mineral oil T=0°C; 0.5 h; 2: chloromethyl methyl ether in tetrahydrofuran; mineral oil T=0 - 20°C;
参考文献
European Journal of Organic Chemistry, , # 24 p. 4654 - 4666
反应条件
in dichloromethane T=25°C; Rate constantEquilibrium constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 8 p. 1543 - 1551
Zhurnal Organicheskoi Khimii, , vol. 20, # 8 p. 1695 - 1704
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine
1.) Et2O, 14 deg C, 1 h, 2.) -78 deg C -> 14 deg C; 14 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Chadwick, Derek J.; Ngochindo, Raphael I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 481 - 486
反应条件
triethylamine in acetonitrile
15 h; Ambient temperature;
参考文献
Regel,E.
Justus Liebigs Annalen der Chemie, 1977 , p. 159 - 168
