2-(苯基甲基)-1,3-苯并恶唑合成路线 (共 32 条)
反应条件
1,3,2-benzodithiazole 1,1,3,3-tetraoxide in neat (no solvent)
T=20 - 25°C; 3 h; Green chemistry;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
Arkivoc, 2012 , vol. 2012, # 9 p. 262 - 279
反应条件
1,4-diaza-bicyclo[2.2.2]octane in 1-methyl-pyrrolidin-2-one
T=100°C; 10 h;
参考文献
Tao, Kemei; Zheng, Jianlong; Liu, Zhaogui; Shen, Wang; Zhang, Jiancun
Tetrahedron Letters, 2010 , vol. 51, # 24 p. 3246 - 3249
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in toluene
T=215°C; 5 h;
参考文献
Kondo, Teruyuki; Yang, Sungbong; Huh, Keun-Tae; Kobayashi, Masanobu; Kotachi, Shinji; Watanabe, Yoshihisa
Chemistry Letters, 1991 , p. 1275 - 1278
反应条件
copper(II) bis(trifluoromethanesulfonate) in chlorobenzene
5 h; Reflux;
参考文献
Tan, Heng; Pan, Cheng-Xue; Xu, Yan-Li; Wang, Heng-Shan; Pan, Ying-Ming
Journal of Chemical Research, 2012 , vol. 36, # 6 p. 370 - 373
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; sodium acetate in dimethyl sulfoxide
T=120°C; 3 h; Inert atmosphere;
参考文献
Mukai, Tomoya; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2010 , vol. 12, # 6 p. 1360 - 1363
反应条件
copper(l) iodide; lithium tert-butylate in 1,4-dioxane
T=120°C; 1.5 h; Inert atmosphere;
参考文献
Zhao, Xia; Wu, Guojiao; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 10 p. 3296 - 3299
反应条件
potassium phosphate; 1,3-bis-(diphenylphosphino)propane; palladium diacetate in N,N-dimethyl-formamide
T=120°C; 16 h; chemoselective reaction;
参考文献
Xie, Pan; Huang, Hanmin; Xie, Yinjun; Guo, Shengmei; Xia, Chungu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1692 - 1700
反应条件
potassium phosphate; palladium (II) trifluoroacetate; 1,3-bis-(diphenylphosphino)propane in N,N-dimethyl-formamide
T=120°C; 16 h; Inert atmosphere; chemoselective reaction;
参考文献
Xie, Pan; Huang, Hanmin; Xie, Yinjun; Guo, Shengmei; Xia, Chungu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1692 - 1700
反应条件
palladous nitrate
T=120°C; 24 h;
参考文献
Shimada, Tomohiro; Yamamoto, Yoshinori
Journal of the American Chemical Society, 2003 , vol. 125, # 22 p. 6646 - 6647
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; bis(1,2-diphenylphosphino)benzene in chlorobenzene
6 h; Inert atmosphereReflux;
参考文献
Li, Guangzhe; Arisawa, Mieko; Yamaguchi, Masahiko
Chemical Communications, 2014 , vol. 50, # 33 p. 4328 - 4330