反应条件
1: 1. t-BuOK / 1. THF, -30 deg C, 15 min, 2. THF, a. -78 deg C, 3 h, b. r.t., 15 h 2: 92 percent / KOH / methanol; H2O / 1. 55 deg C, 7 h, 2. r.t., 15 h 3: 71 percent / Pb(OAc)4, Cu(OAc)2*H2O, pyridine / benzene / 2 h / Heating 4: 1. 9-BBN, 2. 3N NaOH, 26percent H2O2 / 1. THF, r.t., 5 h, 2. r.t., 17 h View Scheme
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Khasanov, Kh. D.; Abduvakhabov, A. A.; Tolstikov, G. A.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 116 - 118
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 132 - 135
