六氟-2-(对甲苯基)异丙醇合成路线 （共 7 条）
反应条件
aluminium trichloride
参考文献
Journal of the American Chemical Society, , vol. 87, # 11 p. 2410 - 2420
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 591 - 595
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 614 - 618
反应条件
iodine; magnesium 1.) ether, reflux; 2.) ether, overnight; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 108, # 12 p. 3470 - 3474
反应条件
1: SF4 / Heating 2: (i) Br2, (irradiation), (ii) HNO3 View Scheme
参考文献
Sheppard,W.A.
Journal of the American Chemical Society, 1965 , vol. 87, # 11 p. 2410 - 2420
反应条件
nitric acid T=180 - 185°C;
参考文献
Livshits,B.R. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 591 - 595
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , # 3 p. 614 - 618
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane T=20°C; 50 h; Heating / reflux;
参考文献
PHARMACIA CORPORATION
Patent: WO2003/99775 A1, 2003 ;
Location in patent: Page 16 ;
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane T=80°C; 2 h;
参考文献
GAWECO, Anderson; TILLEY, Jefferson, W.; WALKER, John; PALMER, Samantha; BLINN, James
Patent: WO2013/166013 A1, 2013 ;
Location in patent: Paragraph 0085 ;
反应条件
(i) SF4, (ii) NaF, CH2Cl2; Multistep reaction;
参考文献
Sheppard,W.A.
Journal of the American Chemical Society, 1965 , vol. 87, # 11 p. 2410 - 2420
