2-苄氧基-3-甲氧基苯甲醛合成路线 （共 13 条）
反应条件
1: 94 percent / diethyl ether / 0.5 h / Ambient temperature
2: 93 percent / PCC/Al2O3, NaOAc / CH2Cl2 / Heating
View Scheme
参考文献
Selfridge, Brandon R.; Deschamps, Jeffrey R.; Jacobson, Arthur E.; Rice, Kenner C.
Journal of Organic Chemistry, 2014 , vol. 79, # 11 p. 5007 - 5018
反应条件
1: sodium tetrahydroborate / 1 h / 0 - 20 °C
2: phosphorus tribromide / 1,4-dioxane / 1 h / 40 °C
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参考文献
Kanekar, Yogesh; Basha, Khalander; Duche, Sharad; Gupte, Rajan; Kapat, Arnab
European Journal of Medicinal Chemistry, 2013 , vol. 67, p. 454 - 463
反应条件
1: 94 percent / diethyl ether / 0.5 h / Ambient temperature
2: 93 percent / PCC/Al2O3, NaOAc / CH2Cl2 / Heating
3: 93 percent / glacial AcOH, NaCNBH3, MgSO4 / methanol / 9 h / Heating
4: 1.) 4N aq. HCl, 2.) H2 / 2.) 10percent Pd/C / 1.) RT, overnight, 2.) 1 atm, 24 h
View Scheme
参考文献
Kaufman
Synthetic Communications, 1992 , vol. 22, # 13 p. 1913 - 1921
