1,2-二(2-羟基苯氧基)乙烷合成路线 （共 16 条）
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate T=25°C; P=2280 Torr; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 56, # 3 p. 1236 - 1242
反应条件
2,4,6-trimethyl-pyridine; lithium iodide T=150°C; 3 h; Inert atmosphere;
参考文献
ARKIVOC (Gainesville, FL, United States), , vol. 2010, # 7 p. 217 - 237,21
反应条件
1: KOH / ethanol 2: H2 View Scheme
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 58, # 9 p. 838 - 842
反应条件
1.1: caesium carbonate / acetonitrile / 3 h / 20 °C / |Inert atmosphere; |Reflux 1.2: 24 h / |Inert atmosphere; |Reflux 2.1: 2,4,6-trimethyl-pyridine; lithium iodide / 3 h / 150 °C / |Inert atmosphere View Scheme
参考文献
ARKIVOC (Gainesville, FL, United States), , vol. 2010, # 7 p. 217 - 237,21
反应条件
1.1: caesium carbonate / acetonitrile / 3 h / |Inert atmosphere; |Reflux 1.2: |Inert atmosphere; |Reflux 2.1: hydrogenchloride / dichloromethane; methanol; water View Scheme
参考文献
ARKIVOC (Gainesville, FL, United States), , vol. 2010, # 7 p. 217 - 237,21
反应条件
(i) NaH, DMF, (ii) aq. AcOH; Multistep reaction;
参考文献
Journal of Medicinal Chemistry, , vol. 21, p. 357 - 361
参考文献
Magnetic Resonance in Chemistry, , vol. 26, p. 387 - 391
反应条件
potassium hydroxide in dimethyl sulfoxide T=90°C; 2.5 h;
参考文献
Kotlyar; Gorodnyuk; Grigorash; Chuprin
Russian Journal of General Chemistry, 1998 , vol. 68, # 7 p. 1135 - 1138
反应条件
1: 2,2'-lt;1,2-ethanediylbis(oxy)gt;bisphenol With caesium carbonate in acetonitrile 3 h; RefluxInert atmosphere; 2: 2,2'-(2,2'-oxybis(ethan-2,1-diyl)bis(oxy))bis(ethan-2,1-diyl)dimethansulfonate in acetonitrile Inert atmosphereReflux;
参考文献
Hanes, Robert E.; Lee, Jong Chan; Ivy, Sheryl N.; Palka, Anna; Bartsch, Richard A.
Arkivoc, 2010 , vol. 2010, # 7 p. 238 - 248
反应条件
potassium hydroxide in dimethyl sulfoxide T=90°C; 2.5 h;
参考文献
Kotlyar; Gorodnyuk; Grigorash; Chuprin
Russian Journal of General Chemistry, 1998 , vol. 68, # 7 p. 1135 - 1138
