2,2-二氯丙二酸二乙酯合成路线 （共 23 条）
反应条件
tris-(dimethylamino)-phosphine in tetrahydrofuran T=-35 - 24°C;
参考文献
Tetrahedron, , vol. 46, # 10 p. 3489 - 3502
反应条件
sodium hypochlorite in acetic acid; acetone
T=0°C; 1 h;
参考文献
Kim, Jeum-Jong; Kweon, Deok-Heon; Cho, Su-Dong; Kim, Ho-Kyun; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synlett, 2006 , # 2 p. 194 - 200
反应条件
lead(IV) acetate; aluminium trichloride in acetonitrile
T=20°C; 2 h;
参考文献
Kim, Jeum-Jong; Kweon, Deok-Heon; Cho, Su-Dong; Kim, Ho-Kyun; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synlett, 2006 , # 2 p. 194 - 200
反应条件
chlorine
T=55 - 60°C;
参考文献
Amriev; Velichko; Abdulkina
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 111 pt 1 p. 2318 - 2322
反应条件
tris-(dimethylamino)-phosphine in tetrahydrofuran
T=-35°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Vorbruggen; Bohn; Krolikiewicz
Tetrahedron, 1990 , vol. 46, # 10 p. 3489 - 3502
参考文献
Conrad; Brueckner
Chemische Berichte, 1891 , vol. 24, p. 3002
反应条件
triethylamine in tetrahydrofuran
T=10 - 50°C; Mechanism; Reagent/catalystSolvent;
参考文献
Shainyan; Danilevich, Yu. S.
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 9 p. 1412 - 1413
反应条件
zinc(II) chloride
T=110 - 120°C;
参考文献
Gross,H.; Freiberg,J.
Chemische Berichte, 1968 , vol. 101, p. 3201 - 3207
反应条件
1: Cl2 / CCl4
2: ZnCl2 / 110 - 120 °C
View Scheme
参考文献
Gross,H.; Freiberg,J.
Chemische Berichte, 1968 , vol. 101, p. 3201 - 3207
参考文献
Conrad; Reinbach
Chemische Berichte, 1902 , vol. 35, p. 1814
