反应条件
in diethyl ether N2-atmosphere; addn. of 2 equiv. diol to B-compd., stirring for at room temp. for 5 h; cooling to -78°C, addn. of excess 1 M HCl in Et2O, slow warming to room temp., solvent removal (vac.), extn. into hexane (Soxhlet), recrystn. (hexane/CH2Cl2=9:1); elem. anal.;
参考文献
Lawlor, Fiona J.; Norman, Nicholas C.; Pickett, Nigel L.; Robins, Edward G.; Nguyen, Paul; Lesley, Gerry; Marder, Todd B.; Ashmore, Jennifer A.; Green, Jennifer C.
Inorganic Chemistry, 1998 , vol. 37, # 20 p. 5282 - 5288
