1-(6-甲基苯并[d]噻唑-2-基)肼合成路线 (共 12 条)
反应条件
hydrogenchloride; hydrazine hydrate in ethylene glycol Microwave irradiation;
参考文献
Munirajasekhar; Himaja; Mali, Sunil V.
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 2 p. 459 - 465
反应条件
1: ammonia; bromine; acetic acid 2: hydrogenchloride; hydrazine hydrate / water; ethylene glycol / Reflux View Scheme
参考文献
Archiv der Pharmazie, , vol. 343, # 11-12 p. 692 - 699
反应条件
hydrazine hydrate in ethanol; water 3 h; Reflux;
参考文献
Chemistry and Biodiversity, , vol. 8, # 2 p. 253 - 265
反应条件
1: Br2 2: NH2NH2 View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 48, # 4 p. 783 - 786
反应条件
1: Br2 2: NH2NH2 View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 48, # 4 p. 783 - 786
参考文献
Vaid, R. K.; Dhindsa, G. S.; Kaushik, B.; Singh, S. P.; Dhawan, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 569 - 570
反应条件
T=160°C; Yield given;
参考文献
Vaid, Radhe K.; Dhindsa, Gurnam S.; Kaushik, Beena; Singh, Shiv P.
Organic Mass Spectrometry, 1987 , vol. 22, p. 36 - 38
反应条件
acetic acid in ethanol 1) reflux, 2) r.t.;
参考文献
Singh, S. P.; Vaid, R. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 288 - 291
反应条件
thionyl chloride T=50°C; 2 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 14 p. 4022 - 4025
反应条件
T=100 - 105°C; P=60 - 65 Torr; 1 h;
参考文献
Zhang, Jing-Lin; Ma, Xiao-Bo
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 53, # 1-4 p. 291 - 298