2-肼基-6-甲氧基-1,3-苯并噻唑合成路线 (共 9 条)
反应条件
hydrogenchloride; hydrazine hydrate in ethylene glycol Microwave irradiation;
参考文献
Munirajasekhar; Himaja; Mali, Sunil V.
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 2 p. 459 - 465
反应条件
1: ammonia; bromine; acetic acid 2: hydrogenchloride; hydrazine hydrate / water; ethylene glycol / Reflux View Scheme
参考文献
Archiv der Pharmazie, , vol. 343, # 11-12 p. 692 - 699
反应条件
hydrazine hydrate in ethanol; water 3 h; Reflux;
参考文献
Chemistry and Biodiversity, , vol. 8, # 2 p. 253 - 265
反应条件
1.1: potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride / acetonitrile / |Reflux 2.1: sulfuric acid / ethylene glycol; water / 0.5 h / 80 °C 2.2: 5 h / 140 °C View Scheme
参考文献
Archiv der Pharmazie, , vol. 347, # 4 p. 268 - 275
反应条件
1: Br2 2: NH2NH2*H2O View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 66, p. 39 - 41
参考文献
Vaid, R. K.; Dhindsa, G. S.; Kaushik, B.; Singh, S. P.; Dhawan, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 569 - 570
反应条件
T=160°C; Yield given;
参考文献
Vaid, Radhe K.; Dhindsa, Gurnam S.; Kaushik, Beena; Singh, Shiv P.
Organic Mass Spectrometry, 1987 , vol. 22, p. 36 - 38
反应条件
acetic acid in ethanol 1) reflux, 2) r.t.;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 25, p. 288 - 291
反应条件
thionyl chloride T=50°C; 2 h;
参考文献
Ouyang, Liang; Huang, Yuhui; Zhao, Yuwei; He, Gu; Xie, Yongmei; Liu, Jie; He, Jun; Liu, Bo; Wei, Yuquan
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 9 p. 3044 - 3049