2-(4-甲基-1,3-二恶烷-4-基)乙醇合成路线 （共 6 条）
反应条件
1: 61 percent / SOCl2, pyridine / 20 °C 2: 87 percent / NaNO2, 50percent nitric acid / 5 h / 40 - 45 °C 3: 60 percent / K2CO3, Katamin AB / acetone / 3 h / 40 - 45 °C 4: 76 percent / NaNO2, 50percent nitric acid / 5 h / 35 - 40 °C View Scheme
参考文献
Sargsyan, M. S.; Manukyan, A. T.; Mkrtumyan, S. A.; Gevorkyan, A. A.
Chemistry of Natural Compounds, 1990 , vol. 26, # 1 p. 24 - 25
Khimiya Prirodnykh Soedinenii, 1990 , # 1 p. 31 - 32
反应条件
nitric acid 1. adding, 7 h; 50-60 deg C, 1 h;
参考文献
Devekki, A. B.; Egor'kov, A. N.; Blanshtein, I. B.; Devekki, A. V.; Idlis, G. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , vol. 24, # 9 p. 1066
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , # 9 p. 1284
反应条件
hydrogen; copper T=240°C; P=225018 Torr; 5 h;
参考文献
Devekki, A. V.; Koshelev, Yu. N.; Malov, Yu. I.; Devekki, A. B.; Strashnova, G. M.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 11 p. 2652 - 2653,2392 - 2393
反应条件
oxalic acid T=150°C; P=4484 Torr; 2.5 h;
参考文献
Russian Journal of General Chemistry, , vol. 64, # 1.2 p. 129 - 131
Zhurnal Obshchei Khimii, , vol. 64, # 1 p. 139 - 141
反应条件
1: 61 percent / SOCl2, pyridine / 20 °C 2: 87 percent / NaNO2, 50percent nitric acid / 5 h / 40 - 45 °C 3: 60 percent / K2CO3, Katamin AB / acetone / 3 h / 40 - 45 °C View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 26, # 1 p. 24 - 25
Khimiya Prirodnykh Soedinenii, , # 1 p. 31 - 32
反应条件
nitric acid
1. adding, 7 h; 50-60 deg C, 1 h;
参考文献
Devekki, A. B.; Egor'kov, A. N.; Blanshtein, I. B.; Devekki, A. V.; Idlis, G. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , vol. 24, # 9 p. 1066
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , # 9 p. 1284
