反应条件
1: 49 percent / Al2(SO4)3 / octane / 78 °C
2: 1.) oxalyl chloride, dimethyl sulfoxide, 2.) Me3N / 1.) CH2Cl2, -78 deg C, 25 min, 2.) 15 min
3: 76 percent / tetrahydrofuran / 0.5 h / 0 °C
4: 95 percent / i-Pr2NEt / CH2Cl2 / 1 h / 0 °C
5: 97 percent / LiAlH4 / tetrahydrofuran / 3 h / 80 °C
6: 98 percent / pyridinium p-toluene sulfonate / ethanol / 8 h / 60 °C
View Scheme
参考文献
Fukuda, Hiroshi; Kitazume, Tomoya
Journal of Fluorine Chemistry, 1995 , vol. 74, # 2 p. 171 - 176
