(S)-(-)-2,3-二苄氧基-1-丙醇合成路线 （共 23 条）
反应条件
1: (i) KOH, (ii) aq. AcOH, (iii) Pb(OAc)4, benzene
2: LiAlH4 / diethyl ether / Heating
View Scheme
参考文献
Eibl,H.; Westphal,O.
Justus Liebigs Annalen der Chemie, 1970 , vol. 738, p. 161 - 169
反应条件
hydrogenchloride in methanol
参考文献
Uzawa, Hirotaka; Nishida, Yoshihiro; Ohrui, Hiroshi; Meguro, Hiroshi
Agricultural and Biological Chemistry, 1989 , vol. 53, # 9 p. 2327 - 2334
反应条件
formic acid; sulfuric acid
1.) 100 deg C, 1 h; 2.) 100 deg C, 14 h; Yield given. Multistep reaction;
参考文献
Andguladze, M. K.; Kaplun, A. P.; Kulish, M. A.; Shvets, V. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 846 - 851
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 5 p. 954 - 961
反应条件
sodium tetrahydroborate; sodium periodate
1.) methanol/water, 20 deg C, 2 h, 2.) methanol, 1 h; Yield given. Multistep reaction;
参考文献
Boeckel, C. A. A. van; Visser, G. M.; Boom, J. H. van
Tetrahedron, 1985 , vol. 41, # 20 p. 4557 - 4566
反应条件
formic acid; sulfuric acid
Yield given. Multistep reaction;
参考文献
Andguladze, M. K.; Kaplun, A. P.; Kulish, M. A.; Shvets, V. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 846 - 851
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 5 p. 954 - 961
反应条件
formic acid; sulfuric acid
1.) 100 deg C, 1 h; 2.) 100 deg C, 14 h; Yield given. Multistep reaction;
参考文献
Anguladze, M. K.; Kaplun, A. P.; Shvets, V. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2075 - 2080
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2323 - 2329
Title/Abstract Full Text Show Details
Andguladze, M. K.; Kaplun, A. P.; Kulish, M. A.; Shvets, V. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 846 - 851
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 5 p. 954 - 961
反应条件
1: 1.) sodium hydride, imidazole / 1.) dimethylformamide, 2.) dimethylformamide, 20 deg C, 15 h
2: 58 percent / aq. acetic acid / 3 h / 100 °C
3: 1.) lead(IV) acetate, 2.) sodium borohydride, aq. NaOH / 1.) THF, 20 deg C, 2.) THF, from 0 deg C to 20 deg C, 2.5 h
View Scheme
参考文献
McAdam, David P.; Perera, Anna M. A.; Stick, Robert V.
Australian Journal of Chemistry, 1987 , vol. 40, # 11 p. 1901 - 1908
反应条件
1: 58 percent / aq. acetic acid / 3 h / 100 °C
2: 1.) lead(IV) acetate, 2.) sodium borohydride, aq. NaOH / 1.) THF, 20 deg C, 2.) THF, from 0 deg C to 20 deg C, 2.5 h
View Scheme
参考文献
McAdam, David P.; Perera, Anna M. A.; Stick, Robert V.
Australian Journal of Chemistry, 1987 , vol. 40, # 11 p. 1901 - 1908
反应条件
Alkaline; water
Multistep reaction;
参考文献
Andguladze, M. K.; Kaplun, A. P.; Kulish, M. A.; Shvets, V. I.; Evstigneeva, R. P.
Doklady Chemistry, 1982 , vol. 263, p. 138 - 139
Dokl. Akad. Nauk SSSR Ser. Khim., 1982 , vol. 263, # 6 p. 1377 - 1379
反应条件
Alkaline; water
Multistep reaction;
参考文献
Andguladze, M. K.; Kaplun, A. P.; Kulish, M. A.; Shvets, V. I.; Evstigneeva, R. P.
Doklady Chemistry, 1982 , vol. 263, p. 138 - 139
Dokl. Akad. Nauk SSSR Ser. Khim., 1982 , vol. 263, # 6 p. 1377 - 1379
