3-05-00-02461 (Beilstein Handbook Reference)合成路线 （共 7 条）
反应条件
Yield given. Multistep reaction;
参考文献
Harvey, Ronald G.; Abu-shqara, Elias; Yang, ChengXi
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6313 - 6317
反应条件
potassium hydroxide; hydrazine hydrate in ethylene glycol
T=175°C;
参考文献
Lee-Ruff, Edward; Kruk, Henry; Katz, Morris
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 553 - 555
反应条件
methanesulfonic acid; palladium on activated charcoal
1.) CH2Cl2, 0 deg C, 30 min, 2.) triglyme, reflux, 30 min; Yield given. Multistep reaction;
参考文献
Harvey, Ronald G.; Pataki, John; Cortez, Cecilia; Raddo, Pasquale Di; Yang, ChengXi
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 1210 - 1217
反应条件
1: 65 percent / HF / 1.) -75 deg C, 1 h, 2.a) 0 deg C, b) room temp.
2: 60 percent / hydrazine hydrate, KOH / ethane-1,2-diol / 175 °C
View Scheme
参考文献
Lee-Ruff, Edward; Kruk, Henry; Katz, Morris
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 553 - 555
反应条件
1: 92 percent / HF / CH2Cl2 / 24 h / Ambient temperature
2: N2H4 / bis-(2-hydroxy-ethyl) ether / 2 h / 140 °C
3: aq. NaOH / bis-(2-hydroxy-ethyl) ether / 10 h / Heating
View Scheme
参考文献
Dai, Wei; Harvey, Ronald G.
Organic Preparations and Procedures International, 1997 , vol. 29, # 3 p. 347 - 352
参考文献
Nagel; Kupper; Antonson; Wallcave
The Journal of organic chemistry, 1977 , vol. 42, # 22 p. 3626 - 3628
反应条件
multistep reaction, new general synthesis of polycyclic aromatic compounds based on enamine chemistry;
参考文献
Harvey, Ronald G.; Pataki, John; Cortez, Cecilia; Raddo, Pasquale Di; Yang, ChengXi
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 1210 - 1217
