1,3,3-三甲基-2,3-二氢-1H-吲哚-2-酮合成路线 （共 67 条）
反应条件
methanol; sodium methylate
T=100 - 120°C;
参考文献
Brunner
Monatshefte fuer Chemie, 1897 , vol. 18, p. 115,116
Monatshefte fuer Chemie, 1895 , vol. 16, p. 864
反应条件
1: POCl3 / dioxane / 4 h / 80 °C
2: aq. NaOH / Ambient temperature
View Scheme
参考文献
Kon'kov, L. I.; Przhiyalgovskaya, N. M.; Suvorov, N. N.
Doklady Chemistry, 1984 , vol. 278, p. 350 - 352
Dokl. Akad. Nauk SSSR Ser. Khim., 1984 , vol. 278, # 5 p. 1130 - 1133
反应条件
1: POCl3 / dioxane / 4 h / 80 °C
2: aq. NaOH / Ambient temperature
View Scheme
参考文献
Kon'kov, L. I.; Przhiyalgovskaya, N. M.; Suvorov, N. N.
Doklady Chemistry, 1984 , vol. 278, p. 350 - 352
Dokl. Akad. Nauk SSSR Ser. Khim., 1984 , vol. 278, # 5 p. 1130 - 1133
反应条件
1: POCl3 / dioxane / 4 h / 80 °C
2: aq. NaOH / Ambient temperature
View Scheme
参考文献
Kon'kov, L. I.; Przhiyalgovskaya, N. M.; Suvorov, N. N.
Doklady Chemistry, 1984 , vol. 278, p. 350 - 352
Dokl. Akad. Nauk SSSR Ser. Khim., 1984 , vol. 278, # 5 p. 1130 - 1133
反应条件
1: POCl3 / dioxane / 4 h / 80 °C
2: aq. NaOH / Ambient temperature
View Scheme
参考文献
Kon'kov, L. I.; Przhiyalgovskaya, N. M.; Suvorov, N. N.
Doklady Chemistry, 1984 , vol. 278, p. 350 - 352
Dokl. Akad. Nauk SSSR Ser. Khim., 1984 , vol. 278, # 5 p. 1130 - 1133
反应条件
1: POCl3 / dioxane / 4 h / 80 °C
2: aq. NaOH / Ambient temperature
View Scheme
参考文献
Kon'kov, L. I.; Przhiyalgovskaya, N. M.; Suvorov, N. N.
Doklady Chemistry, 1984 , vol. 278, p. 350 - 352
Dokl. Akad. Nauk SSSR Ser. Khim., 1984 , vol. 278, # 5 p. 1130 - 1133
反应条件
1: POCl3 / dioxane / 4 h / 80 °C
2: aq. NaOH / Ambient temperature
View Scheme
参考文献
Kon'kov, L. I.; Przhiyalgovskaya, N. M.; Suvorov, N. N.
Doklady Chemistry, 1984 , vol. 278, p. 350 - 352
Dokl. Akad. Nauk SSSR Ser. Khim., 1984 , vol. 278, # 5 p. 1130 - 1133
反应条件
1: 80 percent / NaH / tetrahydrofuran / Ambient temperature
2: 72 percent Spectr. / tri-n-butylstannane, AIBN / toluene / Heating
View Scheme
参考文献
Jones, Keith; Thompson, Mervyn; Wright, Colin
Journal of the Chemical Society, Chemical Communications, 1986 , # 2 p. 115 - 116
反应条件
1: 90 percent / diethyl ether / 0 °C
2: 80 percent / NaH / tetrahydrofuran / Ambient temperature
3: 72 percent Spectr. / tri-n-butylstannane, AIBN / toluene / Heating
View Scheme
参考文献
Jones, Keith; Thompson, Mervyn; Wright, Colin
Journal of the Chemical Society, Chemical Communications, 1986 , # 2 p. 115 - 116
反应条件
1.1: sodium hydride / hexane; tetrahydrofuran / 1 h / 20 °C / |Schlenk technique
1.2: 70 °C / |Schlenk technique
2.1: 1,2-diamino-benzene; copper(I) oxide; sodium t-butanolate / tert-butyl alcohol / 48 h / 100 °C / |Sealed tube
View Scheme
参考文献
Jhan, Yu-Huei; Kang, Ting-Wei; Hsieh, Jen-Chieh
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1155 - 1159
