1,3,3-三甲基-2,3-二氢-1H-吲哚-2-酮合成路线 (共 67 条)
反应条件
sodium hydroxide; trichlorophosphate
1. dioxane, 80 degC, 4h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Prizhiyalgovskaya, N. M.; Kon'kov, L. I.; Tarshits, D. L.; Salmina, S. V.; Segizova, N. T.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 7 p. 751 - 754
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 7 p. 915 - 918
反应条件
sodium hydroxide; trichlorophosphate
1. dioxane, 80 degC, 4h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Prizhiyalgovskaya, N. M.; Kon'kov, L. I.; Tarshits, D. L.; Salmina, S. V.; Segizova, N. T.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 7 p. 751 - 754
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 7 p. 915 - 918
反应条件
sodium hydroxide; trichlorophosphate
1. dioxane, 80 degC, 4h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Prizhiyalgovskaya, N. M.; Kon'kov, L. I.; Tarshits, D. L.; Salmina, S. V.; Segizova, N. T.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 7 p. 751 - 754
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 7 p. 915 - 918
反应条件
in acetonitrile
T=13°C; Irradiationphotodecomposition and singlet oxygen production during photosensitization; Product distribution;
参考文献
Salemi-Delvaux, Christiane; Luccioni-Houze, Barbara; Baillet, Gilles; Giusti, Gerard; Guglielmetti, Robert
Tetrahedron Letters, 1996 , vol. 37, # 29 p. 5127 - 5130
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride
T=100°C; Rearrangement; Product distribution; Further Variations:Temperatures;
参考文献
Jones, Keith; Brunton, Shirley A.; Gosain, Rajendra
Tetrahedron Letters, 1999 , vol. 40, # 50 p. 8935 - 8938
参考文献
Piccinini
Gazzetta Chimica Italiana, 1898 , vol. 28 II, p. 59
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1898 , vol. <5> 7 I, p. 363
反应条件
in acetonitrile
T=13°C; Irradiationphotodecomposition and singlet oxygen production during photosensitization; Product distribution;
参考文献
Salemi-Delvaux, Christiane; Luccioni-Houze, Barbara; Baillet, Gilles; Giusti, Gerard; Guglielmetti, Robert
Tetrahedron Letters, 1996 , vol. 37, # 29 p. 5127 - 5130
反应条件
oxygen in acetonitrile
Irradiationsinglet oxygen quenching rate constant in CH2Cl2 at 25 deg C; Mechanism;
参考文献
Malatesta; Milosa; Millini; Lanzini; Bortolus; Monti
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1994 , vol. 246, p. 303 - 310
反应条件
oxygen in acetonitrile
Irradiationsinglet oxygen quenching rate constant in CH2Cl2 at 25 deg C; Mechanism;
参考文献
Malatesta; Milosa; Millini; Lanzini; Bortolus; Monti
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1994 , vol. 246, p. 303 - 310
参考文献
Brunner
Monatshefte fuer Chemie, 1896 , vol. 17, p. 484