3-(2-噻吩基)-DL-丙氨酸合成路线 (共 26 条)
反应条件
1: aq. NaOH solution 2: ethanol; hydroxylamine 3: ethanol; sodium-amalgam View Scheme
参考文献
Journal of Organic Chemistry, , vol. 15, p. 81,87
反应条件
barium dihydroxide; water
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 98; engl. Ausg. S. 89
反应条件
1: sodium-amalgam; ethanol 2: barium hydroxide; water View Scheme
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 98; engl. Ausg. S. 89
反应条件
1: 97 percent / 2 N aq. NaOH / dioxane / 4 h / 50 °C View Scheme
参考文献
Bladon, Christine M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 4 p. 1151 - 1158
反应条件
1: 97 percent / 2 N aq. NaOH / dioxane / 4 h / 50 °C View Scheme
参考文献
Lipkowski, Andrzej W.; Flouret, George
Polish Journal of Chemistry, 1980 , vol. 54, # 11/12 p. 2225 - 2228
反应条件
phenylalanine ammonia-lyase in various solvent(s) T=30°C; pH=8.8; 48 h;
参考文献
Paizs, Csaba; Katona, Adrian; Retey, Janos
Chemistry - A European Journal, 2006 , vol. 12, # 10 p. 2739 - 2744
反应条件
Taxus phenylalanine aminomutase enzyme in water; glycerol T=31°C; pH=8; 20 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Cox, Brad M.; Bilsborrow, Joshua B.; Walker, Kevin D.
Journal of Organic Chemistry, 2009 , vol. 74, # 18 p. 6953 - 6959
反应条件
phenylalanine ammonia-lyase in various solvent(s) T=30°C; pH=8.8; Enzyme kinetics;
参考文献
Weiser, Diana; Varga, Andrea; Kovacs, Klaudia; Nagy, Flora; Szilagyi, Andras; Vertessy, Beata G.; Paizs, Csaba; Poppe, Laszlo
ChemCatChem, 2014 , vol. 6, # 5 p. 1463 - 1469
反应条件
alanine racemase (accession number AE015451 range 4,245,041-4,246,270), cloned from the genome of Pseudomonas putida (KT2440); Taxus phenylalanine aminomutase enzyme in water; glycerol T=31°C; pH=8; 20 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Cox, Brad M.; Bilsborrow, Joshua B.; Walker, Kevin D.
Journal of Organic Chemistry, 2009 , vol. 74, # 18 p. 6953 - 6959
反应条件
Taxus phenylalanine aminomutase enzyme in water; glycerol T=31°C; pH=8; 20 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Cox, Brad M.; Bilsborrow, Joshua B.; Walker, Kevin D.
Journal of Organic Chemistry, 2009 , vol. 74, # 18 p. 6953 - 6959