反应条件
1: 5-fluoro-cytosine With chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane in toluene T=110°C; 0.5 h; 2: 1,2,3-Tri-O-acetyl-5-deoxy-D-ribofuranose With tin(IV) chloride in dichloromethane T=0 - 30°C; 3: With water; sodium hydrogencarbonate in dichloromethane 2 h;
参考文献
DR. REDDY'S LABORATORIES LTD.; DR. REDDY'S LABORATORIES, INC.; KADABOINA, Rajasekhar; NARIYAM, Sekhar, Munaswamy; MURKI, Veerender; VINJAMURI, Raghupati, Rama; BENDA, Srinivas; KOMATI, Shravan, Kumar; GUNDA, Nageshwar
Patent: WO2010/65586 A2, 2010 ;
Location in patent: Page/Page column 23 ;