in acetonitrile Ambient temperatureLiClO4 electrolyte, glassy carbon cathode, Pt anode, -1,0 V potential;

1: 38 percent / acetonitrile / Ambient temperature; LiClO4 electrolyte, glassy carbon cathode, Pt anode, -1,0 V potential 2: 42 percent / acetonitrile / Ambient temperature; LiClO4 electrolyte, glassy carbon cathode, Pt anode, -1,0 V potential 3: 43 percent / acetonitrile / Ambient temperature; LiClO4 electrolyte, glassy carbon cathode, Pt anode, -1,0 V potential 4: 24 percent / acetonitrile / Ambient temperature; LiClO4 electrolyte, glassy carbon cathode, Pt anode, -1,0 V potential 5: 40 percent / acetonitrile / Ambient temperature; LiClO4 electrolyte, glassy carbon cathode, Pt anode, -1,0 V potential View Scheme

Irradiation;

Irradiation;

1: 1) ZnCl2; 2) H3O(1+) / 1) diethyl ether 2: OH(1-) / diethyl ether View Scheme

1.) hexane/ether, -50°C, 4h; 2.) room temp., 16h, hydrolysis; Yield given. Multistep reaction;

1.) hexane/ether, -50°C, 4h; 2.) room temp., 16h, hydrolysis; Yield given. Multistep reaction;

1.) hexane/ether, -50°C, 4h; 2.) room temp., 16h, hydrolysis; Yield given. Multistep reaction;

1.) hexane/ether, -50°C, 4h; 2.) room temp., 16h, hydrolysis; Yield given. Multistep reaction;