4,4'-二硝基-1,1'-联苯-2,2'-二羧酸合成路线 （共 18 条）
反应条件
sulfuric acid; nitric acid T=-15 - 28°C; 24 h;
参考文献
ROLIC AG; CHAPPELLET, Sabrina; ECKERT, Jean-François; IBN-ELHJ, Mohammed; KANNOOKADAN, Valsa; LINCKER, Frédéric; PALIKA, Satish; TANG, Qian; VEENSTRA, Eva
Patent: WO2013/50122 A1, 2013 ;
Location in patent: Page/Page column 99 ;
反应条件
N,N-diethyl-m-phenylenediamine; copper; sodium carbonate weiteres Reagens: Isoamylalkohol;
参考文献
Tuttle
Journal of the American Chemical Society, 1923 , vol. 45, p. 1914
反应条件
durch stark oxydierende Substanzen;
参考文献
Underwood; Kochmann
Journal of the American Chemical Society, 1924 , vol. 46, p. 2073
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Struve
Chemische Berichte, 1877 , vol. 10, p. 75
反应条件
copper T=180 - 210°C; Erhitzen des Reaktionsprodukts mit wss. Essigsaeure unter Zusatz von Schwefelsaeure;
参考文献
Baddar; Gindy
Journal of the Chemical Society, 1948 , p. 1231,1233
反应条件
sulfuric acid; water
参考文献
Ullmann; Bielecki
Chemische Berichte, 1901 , vol. 34, p. 2176
反应条件
dihydrogen peroxide; acetic acid
参考文献
Bochenkov,V.N.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 11 p. 2430 - 2432,2355 - 2357
反应条件
sulfuric acid; nitric acid 2 h; Title compound not separated from byproducts;
参考文献
Rubezhov, Arkadiy
Organic Preparations and Procedures International, 2006 , vol. 38, # 4 p. 401 - 404
反应条件
1: copper powder / 180 - 220 °C 2: concentrated sulfuric acid; water View Scheme
参考文献
Ullmann; Bielecki
Chemische Berichte, 1901 , vol. 34, p. 2176
反应条件
1: HCl 2: copper powder / 180 - 220 °C 3: concentrated sulfuric acid; water View Scheme
参考文献
Ullmann; Bielecki
Chemische Berichte, 1901 , vol. 34, p. 2176
反应条件
1: H2SO4, KNO3 2: aq. H2O2, AcOH View Scheme
参考文献
Bochenkov,V.N.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 11 p. 2430 - 2432,2355 - 2357
