4-羟基-3-硝基香豆素合成路线 (共 14 条)
反应条件
1: trichlorophosphate / N,N-dimethyl-formamide
2: triethylamine / ethanol / Reflux
View Scheme
参考文献
Radulovic, Niko S.; Bogdanovic, Goran A.; Blagojevic, Polina D.; Dekic, Vidosav S.; Vukicevic, Rastko D.
Journal of Chemical Crystallography, 2011 , vol. 41, # 4 p. 545 - 551
反应条件
1: trichlorophosphate / N,N-dimethyl-formamide
2: triethylamine / ethanol / Reflux
View Scheme
参考文献
Radulovic, Niko S.; Bogdanovic, Goran A.; Blagojevic, Polina D.; Dekic, Vidosav S.; Vukicevic, Rastko D.
Journal of Chemical Crystallography, 2011 , vol. 41, # 4 p. 545 - 551
反应条件
10 palladium on activated charcoal; hydrogen in ethanol
T=20°C; 5 h;
参考文献
Matos, Maria Joao; Santana, Lourdes; Uriarte, Eugenio; Serra, Silvia; Corda, Marcella; Fadda, Maria Benedetta; Era, Benedetta; Fais, Antonella
Journal of Pharmacy and Pharmacology, 2012 , vol. 64, # 5 p. 742 - 746
反应条件
1: 65 percent / H2; hydrogen chloride / palladium on activated charcoal / methanol / 3 h
2: 67 percent / aq. NaOH / 2 h / Heating
View Scheme
参考文献
Brady, Ian; Leane, Deirdre; Hughes, Helen P.; Forster, Robert J.; Keyes, Tia E.
Dalton Transactions, 2004 , # 2 p. 334 - 341