5-氨基-1-(苯基甲基)-1H-1,2,3-三唑-4-甲腈合成路线 （共 9 条）
反应条件
potassium carbonate in dimethyl sulfoxide 18 h; Ambient temperature;
参考文献
Cottrell, Ian F.; Hands, David; Houghton, Peter G.; Humphrey, Guy R.; Wright, Stanley H. B.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 2 p. 301 - 304
参考文献
Hoover; Day
Journal of the American Chemical Society, 1956 , vol. 78, p. 5832,5835
反应条件
sodium ethanolate in ethanol Heating;
参考文献
Barili; Biagi; Livi; et al.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 4 p. 997 - 1001
反应条件
hydrogenchloride; trichlorophosphate 1.) DMF, 0 deg C, 5 min, 25 deg C, 10 min, 80 deg C, 15 min, 2.) DMF, water, 80 deg C, 5 min; Yield given. Multistep reaction;
参考文献
L'abbe, Gerrit; Godts, Francoise; Toppet, Suzanne
Bulletin des Societes Chimiques Belges, 1985 , vol. 94, # 7 p. 441 - 448
反应条件
sodium ethanolate in ethanol 4 h; Heating; Product distribution;
参考文献
Barili; Biagi; Livi; et al.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 4 p. 997 - 1001
参考文献
Hoover; Day
Journal of the American Chemical Society, 1956 , vol. 78, p. 5832,5835
反应条件
ethanol; hydrogen sulfide; ammonia
参考文献
Hoover; Day
Journal of the American Chemical Society, 1956 , vol. 78, p. 5832,5835
反应条件
1: 90 percent / pyridine / 1 h / 1 °C
2: 90 percent / 3N NH3 / ethanol / 20 °C
View Scheme
参考文献
Albert, Adrien
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 887 - 891
反应条件
1: 90 percent / pyridine / 1 h / 1 °C
2: 90 percent / 3N NH3 / ethanol / 20 °C
3: 85 percent / 3N NH3, H2 / Raney nickel / ethanol / 18 h / 70 °C / 3040 Torr
View Scheme
参考文献
Albert, Adrien
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 887 - 891
