alpha-苯基-4-硝基苯乙醇合成路线 （共 9 条）
反应条件
sodium tetrahydroborate in methanol 2 h;
参考文献
Wan, Peter; Muralidharan, S.
Journal of the American Chemical Society, 1988 , vol. 110, # 13 p. 4336 - 4345
反应条件
tetrakis(dimethylamino)ethylene in N,N-dimethyl-formamide T=-20 - 20°C; 3 h;
参考文献
Giuglio-Tonolo, Gamal; Terme, Thierry; Medebielle, Maurice; Vanelle, Patrice
Tetrahedron Letters, 2003 , vol. 44, # 34 p. 6433 - 6435
反应条件
1: 1.) thionyl chloride; 2.) AlCl3 / 1.) ca. 55 deg C, 20 min; 2.) refl., 45 min 2: 85 percent / NaBH4 / methanol / 2 h View Scheme
参考文献
Wan, Peter; Muralidharan, S.
Journal of the American Chemical Society, 1988 , vol. 110, # 13 p. 4336 - 4345
反应条件
1: 1.) thionyl chloride; 2.) AlCl3 / 1.) ca. 55 deg C, 20 min; 2.) refl., 45 min 2: 85 percent / NaBH4 / methanol / 2 h View Scheme
参考文献
Wan, Peter; Muralidharan, S.
Journal of the American Chemical Society, 1988 , vol. 110, # 13 p. 4336 - 4345
反应条件
1: With caesium carbonate in tetrahydrofuran; water Suzuki coupling; 15 h; RefluxInert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in tetrahydrofuran; water T=20°C; 2 h; Inert atmosphere;
参考文献
Penno, Dirk; Estevan, Francisco; Fernandez, Elena; Hirva, Pipsa; Lahuerta, Pascual; Sanau, Mercedes; Ubeda, Ma Angeles
Organometallics, 2011 , vol. 30, # 8 p. 2083 - 2094
反应条件
1.1: C62H52N4P2Pd2; sodium acetate / tetrahydrofuran / 4 h / 78 °C / Inert atmosphere 2.1: caesium carbonate / tetrahydrofuran; water / 15 h / Reflux; Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Penno, Dirk; Estevan, Francisco; Fernandez, Elena; Hirva, Pipsa; Lahuerta, Pascual; Sanau, Mercedes; Ubeda, Ma Angeles
Organometallics, 2011 , vol. 30, # 8 p. 2083 - 2094
反应条件
in water; acetonitrile Irradiationprimary isotop effect in D2O, var. pH; Product distributionQuantum yieldMechanism;
参考文献
Wan, Peter; Muralidharan, S.
Journal of the American Chemical Society, 1988 , vol. 110, # 13 p. 4336 - 4345
反应条件
in water; acetonitrile Irradiationprimary isotop effect in D2O, var. pH; Product distributionQuantum yieldMechanism;
参考文献
Wan, Peter; Muralidharan, S.
Journal of the American Chemical Society, 1988 , vol. 110, # 13 p. 4336 - 4345
反应条件
oxygen in water; acetonitrile Irradiation; Product distribution;
参考文献
Wan, Peter; Muralidharan, S.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 1949 - 1952
