3-氮杂-alpha-高-5alpha-胆甾烷-4-酮合成路线 (共 3 条)
反应条件
thionyl chloride in 1,4-dioxane T=40°C; 0.166667 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Dave, Vinod; Stothers, J. B.; Warnhoff, E. W.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 2666 - 2678
反应条件
1: RuO4 / acetic acid; CCl4 / double dosis of INOE 2 and catalyst 2: 91 percent / HONH2*HCl, NaOAc / H2O; methanol / 3 h / Heating 3: p-TsCl, pyridine / 0.5 h / 0 °C View Scheme
参考文献
Dave, Vinod; Stothers, J. B.; Warnhoff, E. W.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 2666 - 2678
反应条件
1: 91 percent / HONH2*HCl, NaOAc / H2O; methanol / 3 h / Heating 2: p-TsCl, pyridine / 0.5 h / 0 °C View Scheme
参考文献
Dave, Vinod; Stothers, J. B.; Warnhoff, E. W.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 2666 - 2678