7-甲氧基-7-氧代庚酸合成路线 （共 27 条）
反应条件
sodium methylate in methanol electrolysis; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 543 - 551
反应条件
sodium methylate in methanol electrolysis; Further byproducts given;
参考文献
Boden, Neville; Bushby, Richard J.; Clark, Leslie D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 543 - 551
反应条件
sodium methylate in methanol electrolysis; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 543 - 551
反应条件
1.1: Et3N; 4-dimethylaminopyridine; dicyclohexylcarbodiimide / CHCl3 / 15 h / 0 - 20 °C 2.1: 67 percent / acetone / toluene / 1.5 h / Heating 3.1: 90 percent / toluene / 1.5 h / Heating 4.1: 73 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C 5.1: 80 percent / NaBH3CN / acetic acid / 5 h / 20 °C 6.1: 89 percent / toluene / Heating 7.1: aq. HCl; NaBH3CN / methanol 7.2: NaOH / H2O; diethyl ether 8.1: SiO2 / toluene / Heating View Scheme
参考文献
Pashkovskii; Katok; Khlebnikova; Koroleva; Lakhvich
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 7 p. 998 - 1009
反应条件
sodium methylate in methanol electrolysis; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 543 - 551
反应条件
sodium hydroxide in water
T=40 - 45°C; electrolysis, carbon electrodes;
参考文献
Misra, R. A.; Sharma, B. L.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 329 - 330
反应条件
1: SOCl2 / 0.75 h / Heating
2: 57 percent / diethyl ether; benzene / 2 h / Heating
View Scheme
参考文献
Dors, Bernhard; Luftmann, Heinrich; Schaefer, Hans J.
Chemische Berichte, 1983 , vol. 116, # 2 p. 761 - 776
