2-甲基-2-丙基4-戊烯-1-基氨基甲酸酯合成路线 （共 54 条）
反应条件
sodium periodate; RuCl3 monohydrate in tetrachloromethane; water; acetonitrile T=20°C; 16 h;
参考文献
Huang, Wei; Ma, Jing-Yi; Yuan, Mu; Xu, Long-Fei; Wei, Bang-Guo
Tetrahedron, 2011 , vol. 67, # 40 p. 7829 - 7837
反应条件
C16H26CuO in 2-methyl-propan-1-ol; toluene
T=25°C; 1 h;
参考文献
Whittaker, Aaron M; Lalic, Gojko
Organic Letters, 2013 , vol. 15, # 5 p. 1112 - 1115
反应条件
triethylamine in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Pavlyuk, Oksana; Teller, Henrik; McMills, Mark C.
Tetrahedron Letters, 2009 , vol. 50, # 23 p. 2716 - 2718
反应条件
n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran
T=-78 - 20°C; Inert atmosphere;
参考文献
Georgiou, Irene; Whiting, Andrew
European Journal of Organic Chemistry, 2012 , # 22 p. 4110 - 4113
反应条件
trifluoroacetic acid in dichloromethane
T=20°C; 20 h;
参考文献
Hodgson, David M.; Reynolds, Nigel J.; Coote, Steven J.
Tetrahedron Letters, 2002 , vol. 43, # 44 p. 7895 - 7897
反应条件
1: di-tert-butyl dicarbonate With triethylamine in dichloromethane
T=0°C; 0.0833333 h; Inert atmosphere;
2: 4-pentenyl-1-amine hydrochloride in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Nicolai, Stefano; Sedigh-Zadeh, Raha; Waser, Jeroime
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3783 - 3801
反应条件
[Co(triphenylphosphane)2Cl2]; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=25°C; 1 h; Inert atmosphere;
参考文献
Hsu, Shih-Fan; Ko, Chih-Wei; Wu, Yao-Ting
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1756 - 1762
反应条件
[Co(triphenylphosphane)2Cl2]; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=25°C; 1 h; Inert atmosphere;
参考文献
Hsu, Shih-Fan; Ko, Chih-Wei; Wu, Yao-Ting
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1756 - 1762
反应条件
1: 4-iodoveratrole With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0); iodine; zinc in N,N-dimethyl-formamide
T=0°C; Negishi coupling reaction; Inert atmosphere;
2: (S)-N-Boc-2-(iodomethyl)pyrrolidine in N,N-dimethyl-formamide
T=0 - 20°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Massah, Ahmad Reza; Ross, Andrew J.; Jackson, Richard F. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8275 - 8278
反应条件
1: 2-iodo-1-lt;(tert-butyloxycarbonyl)aminogt;ethane With chloro-trimethyl-silane; zinc in N,N-dimethyl-formamide
T=0°C;
2: allyl bromide With copper(I) bromide dimethylsulfide complex in N,N-dimethyl-formamide
T=20°C; 14 h; Further stages.;
参考文献
Hunter; Jackson; Rami
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 12 p. 1349 - 1352
