2-甲基-2-丙基4-戊烯-1-基氨基甲酸酯合成路线 （共 54 条）
反应条件
1.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 0 - 20 °C / Inert atmosphere
2.1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0); iodine; zinc / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
View Scheme
参考文献
Massah, Ahmad Reza; Ross, Andrew J.; Jackson, Richard F. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8275 - 8278
反应条件
1.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 0 - 20 °C / Inert atmosphere
2.1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0); iodine; zinc / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
View Scheme
参考文献
Massah, Ahmad Reza; Ross, Andrew J.; Jackson, Richard F. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8275 - 8278
反应条件
palladium diacetate; caesium carbonate; bis[2-(diphenylphosphino)phenyl] ether in 1,4-dioxane
T=100°C; 16 h; Inert atmosphere;
参考文献
Rossiter, Lana M.; Slater, Meagan L.; Giessert, Rachel E.; Sakwa, Samuel A.; Herr, R. Jason
Journal of Organic Chemistry, 2009 , vol. 74, # 24 p. 9554 - 9557
反应条件
Hoveyda-Grubbs catalyst second generation in dichloromethane
T=20°C; 7 h;
参考文献
Fustero, Santos; Jimenez, Diego; Moscardo, Javier; Catalan, Silvia; Del Pozo, Carlos
Organic Letters, 2007 , vol. 9, # 25 p. 5283 - 5286
