5-甲基-2,3-二氢-1H-茚-4-醇合成路线 （共 7 条）
反应条件
hydrogen; palladium on activated carbon in methanol T=55 - 60°C; P=12411.9 - 12929 Torr; 8 h; Product distribution / selectivity;
参考文献
TORRENT PHARMACEUTICALS LTD.
Patent: US2010/168110 A1, 2010 ;
Location in patent: Page/Page column 20 ;
反应条件
hydrogen; palladium on activated carbon in methanol T=55 - 60°C; P=10343.2 - 12929 Torr; 5 h; Product distribution / selectivity;
参考文献
TORRENT PHARMACEUTICALS LTD.
Patent: US2010/168110 A1, 2010 ;
Location in patent: Page/Page column 19 ;
反应条件
gold(III) chloride in acetonitrile T=20°C;
参考文献
Hashmi; Frost; Bats
Journal of the American Chemical Society, 2000 , vol. 122, # 46 p. 11553 - 11554
反应条件
[(tris(1-pyrazolyl)borate)Ru(P(phenyl)3)(CH3CN)2]PF6; water in various solvent(s) T=100°C; 24 h;
参考文献
Odedra, Arjan; Wu, Chang-Jung; Pratap, Taduri Bhanu; Huang, Chun-Wei; Ran, Ying-Fen; Liu, Rai-Shung
Journal of the American Chemical Society, 2005 , vol. 127, # 10 p. 3406 - 3412
反应条件
gold(III) chloride in acetonitrile T=20°C;
参考文献
Hashmi; Frost; Bats
Journal of the American Chemical Society, 2000 , vol. 122, # 46 p. 11553 - 11554
反应条件
trifluoroacetic acid T=25 - 90°C; 6 h;
参考文献
TORRENT PHARMACEUTICALS LTD.
Patent: US2010/168110 A1, 2010 ;
Location in patent: Page/Page column 19-20 ;
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in trifluoroacetic acid T=90°C; 12 h;
参考文献
Kissei Pharmaceutical Co., Ltd.
Patent: EP1471049 A1, 2004 ;
Location in patent: Page 31 ;
