7-甲氧基香豆素-3-羧酸合成路线 （共 20 条）
反应条件
1: 64 percent / 85.5percent KOH / ethanol / 12 h / 110 °C 2: 10ml TFA / 0.08 h / Ambient temperature 3: 12 h / Ambient temperature 4: 10ml H2O View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 219 - 222
反应条件
1: alkali metal carbonate / N,N-dimethyl-formamide / |Reflux 2: lithium hydroxide hydrate / tetrahydrofuran; water / 1 h / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 22 p. 7107 - 7117
反应条件
1: aq. HCl / 2 h / 90 °C 2: aq. NaHCO3 / 5 h / 90 °C / pH 8.3 View Scheme
参考文献
Synthesis, , # 15 p. 2331 - 2334
反应条件
1: 12 h / Ambient temperature 2: 10ml H2O View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 219 - 222
反应条件
1: 10ml TFA / 0.08 h / Ambient temperature 2: 12 h / Ambient temperature 3: 10ml H2O View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 219 - 222
参考文献
Journal of Chemical Research - Part S, , # 6 p. 354 - 355
反应条件
silver carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium (II) bromide in N,N-dimethyl acetamide; toluene
T=150°C; 1 h; Microwave irradiationInert atmosphere;
参考文献
Messaoudi, Samir; Brion, Jean-Daniel; Alami, Mouad
Organic Letters, 2012 , vol. 14, # 6 p. 1496 - 1499
反应条件
1,10-phenanthroline; oxygen; palladium diacetate in N,N-dimethyl-formamide
T=100°C; 24 h; Sealed tube; regioselective reaction;
参考文献
Khoobi, Mehdi; Molaverdi, Fatemeh; Alipour, Masoumeh; Jafarpour, Farnaz; Foroumadi, Alireza; Shafiee, Abbas
Tetrahedron, 2013 , vol. 69, # 52 p. 11164 - 11168
反应条件
1: thionyl chloride; chloroform
2: ethanol
View Scheme
参考文献
Baker; Collis
Journal of the Chemical Society, 1949 , p. Spl. 12, 14
反应条件
thionyl chloride; chloroform
参考文献
Baker; Collis
Journal of the Chemical Society, 1949 , p. Spl. 12, 14
