lithium aluminium tetrahydride in tetrahydrofuran T=-78°C; Reduction; 3 h;
参考文献
Slaughter, Legrande M.; Wolczanski, Peter T.; Klinckman, Thomas R.; Cundari, Thomas R.
Journal of the American Chemical Society, 2000 , vol. 122, # 33 p. 7953 - 7975
in toluene to soln. of DNi complex was added CD3I in the dark; products identified by GC/mass anal.;
参考文献
Darensbourg, Marcetta Y.; Ludwig, Maria; Riordan, Charles G.
Inorganic Chemistry, 1989 , vol. 28, p. 1630 - 1634
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反应条件
in benzene Kinetics; byproducts: C2H6, C2D6; thermolysis at 50-70°C; monitoring by UV-visible spectrophotometry and mass spectrometry;
参考文献
Roy, Sujit; Puddephatt, Richard J.; Scott, John D.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 2121 - 2126