potassium hydroxide in methanol T=20°C; 2 h;

Stage #1: &nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=0 - 20&deg;C;&nbsp;1.25&nbsp;h;&nbsp;<br />Stage #2: <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587194', constants.ctx, '0')">iodine</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '764767', constants.ctx, '0')">bis(trifluoroacetato)-phenyliodine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=0 - 20&deg;C;&nbsp;<br />Stage #3: <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '764767', constants.ctx, '0')">bis(trifluoroacetato)-phenyliodine</a> <br />T=20&deg;C;&nbsp;24&nbsp;h;&nbsp;<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: CH₂Cl₂ / 1.25 h / 20 &deg;C / cooling<br />2: 36.5 g / I₂; PhI(OCOCF₃)2 / 20 &deg;C / cooling<br /> <br /> &nbsp;