3-甲基异唑-4-甲酸乙酯合成路线 (共 8 条)
反应条件
sodium tetrahydroborate in dimethyl sulfoxide T=20°C; 1 h;
参考文献
Synthesis, , # 8 p. 792 - 794
反应条件
triethylamine in toluene; acetonitrile
参考文献
US6316479 B1, ;
US 6316479 B1
反应条件
phenyl isocyanate; triethylamine in benzene
参考文献
Journal of the American Chemical Society, , vol. 89, p. 5461 - 5462
反应条件
hydroxylamine hydrochloride in methanol 1 h; Heating; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Heterocyclic Chemistry, , vol. 28, # 2 p. 453 - 457
反应条件
1: With hydrogenchloride in water 2: With sodium nitrite in water T=0°C; 3: With hypophosphorous ether in water T=0°C; 1.25 h;
参考文献
Polish Journal of Chemistry, , vol. 83, # 5 p. 887 - 893
反应条件
potassium carbonate Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 6, p. 783 - 786
反应条件
1: Py / 3 h 2: aq. K2CO3 / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 6, p. 783 - 786
参考文献
Sugen, Inc.
Patent: US6316479 B1, 2001 ;
US 6316479 B1