Bhatia, Shameem H.; Buckley, David M.; McCabe, Richard W.; Avent, Anthony; Brown, Robert G.; Hitchcock, Peter B.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 3 p. 569 - 574
1: 5 h; Reflux; 2: With ammonia; water in ethanol T=5°C; 0.0833333 h; 3: With hydrogenchloride in water
参考文献
Smith, Alexander M. R.; Rzepa, Henry S.; White, Andrew J. P.; Billen, Denis; Hii, King Kuok
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 3085 - 3096
1: 1) oxalyl chloride, pyridine, 2) pyridine / 1) CH2Cl2, rt, 2.5 h, 2) CH2Cl2, 0 deg C, 1 h, then 0 deg C -> rt, 1 h 2: 70 percent / H2 / 5percent Pd/C / ethyl acetate / 19 h / 760 Torr / Ambient temperature View Scheme
参考文献
Lermer, Leonard; Neeland, Edward G.; Ounsworth, James P.; Sims, Russell J.; Tischler, Samuel A.; Weiler, Larry
Canadian Journal of Chemistry, 1992 , vol. 70, # 5 p. 1427 - 1445