2-氨基-1-苯基-1-丁酮合成路线 （共 8 条）
反应条件
potassium hydroxide; hydrazine hydrate in various solvent(s)
参考文献
Sikkar, Rein; Martinson, Per
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 8 p. 551 - 558
反应条件
sodium hydroxide
T=120°C; 24 h;
参考文献
Nemeth, Janos; Kiss, Arpad; Hell, Zoltan
Tetrahedron Letters, 2013 , vol. 54, # 45 p. 6094 - 6096
反应条件
1: palladium diacetate; trifluoroacetic acid; tert.-butylhydroperoxide / water / 24 h / 40 °C
2: hydrogenchloride / water / 3 h / 125 °C
View Scheme
参考文献
Szabo, Fruzsina; Simko, Daniel; Novak, Zoltan
RSC Advances, 2014 , vol. 4, # 8 p. 3883 - 3886
反应条件
1: dodecanesulphonic acid sodium salt / water / 0.5 h / 20 °C
2: palladium diacetate; trifluoroacetic acid; tert.-butylhydroperoxide / water / 24 h / 40 °C
3: hydrogenchloride / water / 3 h / 125 °C
View Scheme
参考文献
Szabo, Fruzsina; Simko, Daniel; Novak, Zoltan
RSC Advances, 2014 , vol. 4, # 8 p. 3883 - 3886
反应条件
1:
2: With hydrogenchloride
Heating; Further stages.;
参考文献
Peters, Jens-Uwe; Luebbers, Thomas; Alanine, Alexander; Kolczewski, Sabine; Blasco, Francesca; Steward, Lucinda
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 1 p. 256 - 261
反应条件
ethanol; ammonium chloride; zinc
参考文献
Morgan; Hickinbottom
Journal of the Chemical Society, 1921 , vol. 119, p. 1888
反应条件
1: acetic acid anhydride; fuming nitric acid / <5
2: zinc dust; ammonium chloride; alcohol
View Scheme
参考文献
Morgan; Hickinbottom
Journal of the Chemical Society, 1921 , vol. 119, p. 1888
反应条件
Yield given. Multistep reaction;
参考文献
Sikkar, Rein; Martinson, Per
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 8 p. 551 - 558
