3-(2-羟苯基)丙酸甲酯合成路线 （共 14 条）
反应条件
sulfuric acid 5 h; Heating;
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 23, # 1-2 p. 89 - 115
反应条件
palladium 10 on activated carbon; hydrogen in methanol P=1810.07 Torr; 48 h; Inert atmosphere;
参考文献
Williams, John D.; Khan, Atiyya R.; Cardinale, Steven C.; Butler, Michelle M.; Bowlin, Terry L.; Peet, Norton P.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 1 p. 419 - 434
反应条件
1: in toluene T=100°C; Diels-Alder reaction; 2 h; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran T=0°C; 0.0833333 h; Further stages.;
参考文献
Sugimoto, Hiromichi; Nakamura, Satoshi; Ohwada, Tomohiko
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 4-5 p. 669 - 679
参考文献
Barton, Patrick; Laws, Andrew P.; Page, Michael I.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 9 p. 2021 - 2030
反应条件
1.1: TiCl4 / tetrahydrofuran; CCl4 / 2 h / 0 °C 1.2: N-methylmorpholine / tetrahydrofuran; CCl4 / 20 h / 18 °C 2.1: 0.953 g / NaBH4 / CHCl3; propan-2-ol / 4 h / 20 °C 3.1: 83 percent / trifluoromethanesulfonic acid / CHCl3 / 0.5 h / 50 °C 4.1: toluene / 2 h / 100 °C 4.2: 85 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 4-5 p. 669 - 679
反应条件
1.1: 83 percent / trifluoromethanesulfonic acid / CHCl3 / 0.5 h / 50 °C 2.1: toluene / 2 h / 100 °C 2.2: 85 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 4-5 p. 669 - 679
反应条件
1.1: 0.953 g / NaBH4 / CHCl3; propan-2-ol / 4 h / 20 °C 2.1: 83 percent / trifluoromethanesulfonic acid / CHCl3 / 0.5 h / 50 °C 3.1: toluene / 2 h / 100 °C 3.2: 85 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 4-5 p. 669 - 679
反应条件
ammonium cerium(IV) nitrate T=20°C; 24 h;
参考文献
Journal of the Chinese Chemical Society, , vol. 52, # 1 p. 173 - 180
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 407 - 410
反应条件
1.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C / |Inert atmosphere 1.2: 2.08 h / |Inert atmosphere 2.1: hydrogen; palladium 10 on activated carbon / methanol / 48 h / 1810.07 Torr / |Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 22, # 1 p. 419 - 434
