暂无反应条件数据

1: With water; sodium hydroxide in methanol 0.5 h; Reflux; 2: With hydrogenchloride in methanol; water pH=3;

1.1: potassium carbonate; sodium iodide / acetone / 0.08 h / 20 °C / Inert atmosphere 1.2: 24 h / 65 °C 2.1: sodium hydride / ethylene glycol dimethyl ether; mineral oil / 0.17 h / 0 - 20 °C / Inert atmosphere 2.2: 6 h / Reflux 3.1: p-NO2-benzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 3 h / 20 °C 4.1: Rh2[N-[(4-dodecylphenyl)sulfonyl]-(S)-prolinato]4 / toluene / 1.5 h / 0 °C / Inert atmosphere 5.1: chromium(VI) oxide; periodic acid / acetonitrile / 1 h / 20 °C 6.1: water; sodium chloride / dimethyl sulfoxide / 4 h / 155 - 165 °C View Scheme

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C / |Inert atmosphere 1.2: 1 h / 0 - 20 °C / |Inert atmosphere 2.1: potassium hydroxide / methanol / 16 h / 60 °C / |Inert atmosphere View Scheme