DL-β-乙基苯乙基乙醇合成路线 （共 26 条）
反应条件
isopropyl alcohol; zirconium oxide 6 h; Heating;
参考文献
Shibagaki, Makoto; Takahashi, Kyoko; Matasushita, Hajime
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 3283 - 3288
反应条件
1: 44 g / sodium ethoxide / benzene; ethanol / 2 h / Ambient temperature 2: 1.) sodium hydroxide; 2.) 6 N HCl / 1.) H2O, 60 deg C, 2 h; 2.) H2O, reflux, 1 h 3: aluminium isopropoxide, mercuric chloride, isopropanol / 6 h / 110 °C View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 60, # 10 p. 964 - 966
反应条件
T=250°C; P=128714 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 54, p. 4680
反应条件
sodium hydroxide; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; dihydrogen peroxide; 1,4-di(diphenylphosphino)-butane; benzo[1,3,2]dioxaborole 1.) THF, 25 deg C, 4.5 h, 2.) THF, RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Asymmetry, , vol. 2, # 7 p. 601 - 612
反应条件
1: 1.) sodium hydroxide; 2.) 6 N HCl / 1.) H2O, 60 deg C, 2 h; 2.) H2O, reflux, 1 h 2: aluminium isopropoxide, mercuric chloride, isopropanol / 6 h / 110 °C View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 60, # 10 p. 964 - 966
反应条件
1: 1.) Mg 2: LiAlH4 View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 326, # 1 p. 73 - 80
反应条件
1: alcoholic KOH-solution 2: sodium; alcohol; toluene View Scheme
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 184, p. 32
Annales de Chimie (Cachan, France), , vol. <10> 8, p. 281,284
反应条件
ethanol; sodium; toluene
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 184, p. 32
Annales de Chimie (Cachan, France), , vol. <10> 8, p. 281,284
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 184, p. 32
Annales de Chimie (Cachan, France), , vol. <10> 8, p. 281,284
反应条件
n-butyllithium; potassium tert-butylate 1.) THF, hexane, -50 deg C, 5 h, 2.) THF, hexane, from -50 deg C to 20 deg C; Yield given. Multistep reaction;
参考文献
Journal of Chemical Research - Part S, , # 3 p. 158 - 159
